TCC024004 - dsm.pwr.edu.pldsm.pwr.edu.pl/fcp/NGBUKOQtTKlQhbx08... · solid, gas-liquids, liquid...

1

Basic unit processes in chemical technology ............................................................................. 2

Basics of bioinformatics ............................................................................................................. 8

Biochemistry ............................................................................................................................ 12

Chemical Engineering .............................................................................................................. 16

Diffusion Processes .................................................................................................................. 20

Enzymology ............................................................................................................................. 25

Foundations of Chemical Engineering ..................................................................................... 29

Fundamentals in analytical chemistry ...................................................................................... 33

Fundamentals of chemical technology ..................................................................................... 37

Fundamentals of physical chemistry ........................................................................................ 43

Genetic Engineering ................................................................................................................. 48

Heat Transfer Processes ........................................................................................................... 52

Industrial microbiology ............................................................................................................ 57

Information technologies .......................................................................................................... 61

Materials science ...................................................................................................................... 64

Measurements in chemical equipment ..................................................................................... 68

Methods of Materials Testing .................................................................................................. 73

Microbiology II ........................................................................................................................ 77

Organic chemistry .................................................................................................................... 82

Physico-chemical bases of process engineering ....................................................................... 87

Recycling of materials .............................................................................................................. 91

Technical drawing .................................................................................................................... 95

Technical safety ........................................................................................................................ 99

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Zał. nr 4 do ZW 64/2012

Wrocław University of Technology

FACULTY OF CHEMISTRY

SUBJECT CARD

Name in Polish Podstawowe procesy jednostkowe w technologii

chemicznej

Name in English Basic unit processes in chemical technology Main field of study (if applicable) Chemical technology

Specialization (if applicable) Erasmus students

Level and form of studies: 1st level

Kind of subject obligatory

Subject code TCC024004

Group of courses No *delete as applicable

Lecture Classes Laboratory Project Seminar

Number of hours of

organized classes in

University (ZZU) 30

Number of hours of total

student workload (CNPS) 90

Form of crediting Examination For group of courses mark

(X) final course

Number of ECTS points 3 including number of ECTS

points for practical (P) classes

including number of ECTS

points for direct teacher-

student contact (BK) classes 1

*delete as applicable

PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER

COMPETENCES

1. Competence in the field of general and physical chemistry

2. Competence in the field of base mathematics

3.

SUBJECT OBJECTIVES

C1 Introduce students to conception of process and unit operations

C2 Understanding the basic principles of operation of apparatus and reactors for unit

processes and operations in a variety of layouts phase

C3 Introduce students to conception of realization of chemical processes in the

continuous systems

C4 Introduce students to principles of technological systems structure as combination of

chemical unit processes and operations

C5 Acquainting students with the selected processes of chemical technology, non-

catalytic and catalytic processes in a fluidized and stationary beds,

C6 Introduce students to the specific features of biotechnological processes

3

C7 Introduce students to the modern operations of chemical substances operations

SUBJECT EDUCATIONAL EFFECTS

Relating to knowledge:

PEK_W01 – student is able to make the correct characterization of the unit processes and

operations applied in chemical technology,

PEK_W02 – student is able to work up the correct technological scheme of the plant and

select the proper apparatuses and reactors, to indicate the suitable unit

processes and operations,

PEK_W03 – student is able to characterize the flow of chemical substances in various phase

systems

PEK_W04 – student knows the principles of operation of catalytic and non-catalytic

processes and is able to describe and characterize,

PEK_W05 – student obtained the fundamental knowledge on separation technics,

PEK_W06 – student obtained the fundamental knowledge on the methods of biofuels

production,

PEK_W07 – student obtained the fundamental knowledge on polymerization processes and

physicochemical properties the obtained materials,

PEK_W08 – student understands the principles of biotechnological processes.

Relating to skills:

PEK_U01 – student is able to practically work up technological scheme of the process and

define the indispensable unit processes and operations

PEK_U02 – student is able to practically describe the base unit operations and processes for

the selected chemical technologies from the various chemistry branches,

PEK_U03 – student is able to practically realize the simple chemical laboratory as unit

processes and to make the base calculations connected with their realization,

PEK_U04 – student is able to plane and realize the simple separation operation with

application of membrane technics,

PEK_U05 – student is able to determine process effectiveness,

PEK_U06 – student is able to determine physicochemical properties of the obtained reaction

products,

PEK_U07 – student is able to plane and realize the process of chemical modification of raw

materials.

Relating to social competences: PEK_K01

PEK_K02

… change

PROGRAMME CONTENT

Form of classes - lecture Number of hours

Lec 1 The base concepts, unit process, unit operation, definition, characteristics, 2

Lec 2 Scheme of technological process, unit operations and unit processes as

components of chemical technology process. Raw materials, products and

side products of unit operations and processes.

2

Lec 3 Regime and parameters of unit processes and operations. Mixing and 2

4

mass and energy exchange. Equilibrium in chemical processes. Yields and

reagent conversions in unit chemical processes.

Lec 4 Concept of driving reaction force in various flowing systems, methods of

increasing of reaction rate in unit processes. 2

Lec 5 Examples of apparatuses systems for unit processes and operations in gas-

solid, gas-liquids, liquid solids systems, catalytic and non-catalytic three-

phase systems, reactor concepts for various catalyst forms.

2

Lec 6 Examples of chemical technology processes, fluidized bed catalytic

processes, solid bed catalytic processes, 2

Lec 7 Non-catalytic thermal processes, high temperature in heterogeneous

systems, electrolysis processes. 2

Lec 8 Enzymes. Kinetics. Enzymatic processes with native and immobilized

enzyme. 2

Lec 9 Microorganisms, microbiological processes. Kinetics. Products separation. 2

Lec 10 Separation operations: extraction, distillation, chromatography,

sedimentation, flocculation. 2

Lec 11 Ordinary membrane operations, microfiltration, ultrafiltration,

nanofiltration, reversed osmosis, electro-dialysis. 2

Lec 12 Advanced membrane processes, pervaporation, membrane distillation,

membrane pertractors, hybrid processes. 2

Lec 13 Addition polymerization: reaction mechanisms, initiators, inhibitors,

condensation polymerization. 2

Lec 14 Molecular weight. Distribution of molecular weights. Polymer solutions.

Condensed phases. 2

Lec 15 Mixtures. Crystallinity. Phase transformation temperatures.

Total hours 30

Form of classes - class Number of hours

Cl 1

Cl 2

Cl 3

Cl 4

Total hours

Form of classes - laboratory Number of hours

Lab 1 Introductory classes. 2

Lab 2 Catalytic cracking. 4

Lab 3 Rape oil transesterification in flow system. 4

Lab 4 Photodegradation of organic compounds in water. 4

Lab 5 Block polymerization of methyl methacrylate. 4

Lab 6 Membrane separation – isolation of products from reaction mixture. 4

Lab 7 Sulfonation reaction - obtaining of p-toluenesulphonic acid. 4

Lab 8 Alkylation reaction – obtaining of quaternary ammonium salts. 4

Lab 9 or Ions exchange in basic technological processes 4

Total hours 30

5

TEACHING TOOLS USED

N1 Lecture with multimedia presentation

N2 Realization of experimental tasks

N3 Reports from the realized exercises

N4 Consultation

EVALUATION OF SUBJECT EDUCATIONAL EFFECTS ACHIEVEMENT

Evaluation

F – forming (during

semester),

C – concluding (at

semester end)

Educational effect

number Way of evaluating educational effect

achievement

C (lecture)

PEK_W01-

PEK_W08

Final exam

Mark 2.0: 0-50 %

Mark 3.0: 51-60 %

Mark 3.5: 61-70 %

Mark 4.0: 71-80 %

Mark 4.5: 81-90 %

Mark 5.0: 91-98 %

Mark 5.5: >98 %

F1 Laboratory

exercises, preliminary

test

PEK_U02 –

PEK_U08

Partial oral preliminary test (max. 30

points)

F2 Laboratory

exercises, report

PEK_U02 –

PEK_U07

Evaluation of report level (max. 30 points)

C (laboratory exercises) = 3.0 if (F1 + F2)/2= 18.0 – 20 pkt.

3.5 if (F1 + F2)/2 = 20 – 22 pkt.

4.0 if (F1 + F2)/2 = 22 – 24pkt.

4.5 if (F1 + F2)/2 = 24 – 26 pkt.

5.0 if (F1 + F2)/2 = 26 – 28 pkt.

5.5 if (F1 + F2)/2 > 28 pkt.

6

PRIMARY AND SECONDARY LITERATURE

PRIMARY LITERATURE:

[1] I. Mukhlyonov et al. The Theoretical Foundations of Chemical Technology, Part 1 and

Part 2. Mir Publishers, Moscow. 1977.

[2] M. Bodzek, J. Bohodziewicz, K. Konieczny, Techniki membranowe w ochronie

środowiska, Wydawnictwo Politechniki Śląskiej, Gliwice 1997

[3] Praca zbiorowa pod red. Z. Florjańczyka, S. Penczka, Chemia polimerów t. III,

Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa 1998

[4] Szlachta Z., „Zasilanie silników wysokoprężnych paliwami rzepakowymi”, WKŁ

Warszawa 2002.

[5] Baczewski K., Kałdoński T. „Paliwa do silników o zapłonie samoczynnym”, WKŁ

Warszawa 2008

[6] Morrison R.T., Boyd R.N. „Chemia organiczna T.1” Wydawnictwo Naukowe PWN,

Warszawa 2010

SECONDARY LITERATURE:

[1] T. Winnicki, Polimery w ochronie środowiska, Arkady, Warszawa 1978

[2]

[3]

SUBJECT SUPERVISOR

(Prof. dr hab. inż. Jerzy Walendziewski, [email protected])

MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS

FOR SUBJECT

AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY

…………………………………….

Subject

educational

effect

Correlation between subject

educational effect and educational

effects defined for main field of study

and specialization (if applicable)**

Subject

objectives*** Programme

content*** Teaching tool

number***

(knowledge)

PEK_W01 K1Atc_W17 C1 Wy1, Wy2, W3 N1, N4

PEK_W02 K1Atc_W17 C4, C5 Wy3, Wy4, Wy5 N1, N4

PEK_W03 K1Atc_W17 C2, C3, C4 Wy3 - Wy7 N1, N4

PEK_W04 K1Atc_W17 C4, C5 Wy3 - Wy7 N1, N4

PEK_W05 K1Atc_W17 C7 Wy10 –Wy12 N1, N4

PEK_W06 K1Atc_W17 C6 Cw3 N1, N4

PEK_W07 K1Atc_W17 C4 Wy2, Wy3 N1, N4

PEK_W08 K1Atc_W17 C6 Wy13, Wy14 N1, N4

(skills)

PEK_U01 K1Atc_U25 C2, C4 Wy1, Wy2, N3, N4

PEK_U02 K1Atc_U25 C2, C4 Wy6, Wy7 N3, N4

PEK_U03 K1Atc_U25 C7 Cw6 N3, N4

7

PEK_U04 K1Atc_U25 C1, C4 Cw2, Cw3, Cw7 N3, N4

PEK_U05 K1Atc_U25 C3, C5, C7 Cw4, Cw6, Cw8,

Cw9 N3, N4

PEK_U06 K1Atc_U25 C5, C6, C7 Cw3, Cw6, Cw7,

Cw8, Cw9 N3, N4

…

(competences)

PEK_K01

PEK_K02

PEK_K03

…

** - enter symbols for main-field-of-study/specialization educational effects

*** - from table above

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Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Podstawy bioinformatyki

Name in English Basics of bioinformatics Main field of study (if applicable) Biotechnology


Level and form of studies: 1st level, full-time


Subject code BTC013002

Group of courses NO

*delete as applicable Lecture Classes Laboratory Project Seminar

Number of hours of


University (ZZU)

30



Form of crediting Crediting

with grade*

For group of courses mark

(X) final course


points for practical (P) classes 2






COMPETENCES

4. Basic personal computer and internet usage skills

5. Basic knowledge on molecular biology concerning nucleic acids, proteins, genetics

and laboratory techniques

SUBJECT OBJECTIVES

C1 Introduction to basics of programming and algorithms

C2 Introduction to common biomolecular sequence and structure databases

C3 Applications of programming to processing data on biomolecular sequences and

structures

9


Relating to knowledge: Student who completed this course will:

PEK_W01 – know basic instructions and data structures of Python programming language

PEK_W02 – know what is an algorithm, program code, know Python syntax of control

statements and loops

PEK_W03 – knows common sequence and structure databases

PEK_W04 – knows basic sequence and structure file formats

Relating to skills: Student who completed this course can:

PEK_U01 – search sequence and structure databases according to given criteria and

download data in FASTA and PDB formats

PEK_U02 – code simple Python scripts realizing basic bioinformatics tasks, for example

search for restriction sites, transcription, translation, calculation of DNA

melting temperature, calculation of number and lengths of restriction fragments,

introducing mutations

PEK_U03 – code Python programs parsing and saving sequences in FASTA format

PEK_U04 – code Python programs parsing data from PDF files and saving molecular

coordinates in PDB format

PROGRAMME CONTENT


La1 Introduction to Python programming language. First script, operating

system specifics in Windows and Unix. Required software. 3

La2 Interactive work with Python interpreter. Simple data types,

variables. Interactive data input, simple calculations. 3

La3 Python data structures: sequences, indexing and ranges. Operations

on strings of characters. 3

La4 Control statements: conditionals and loops 3

La5 Biological sequence processing: pattern search, melting temperature

calculation, transcription, translation. 3

La6 Python data structures: lists and dictionaries 3

La7 Operation on text files: input, output, data formatting 3

La8 Databases of biological sequences and structures. Common file

formats. 3

La9 Parsing and saving sequences in FASTA format 3

La10 Parsing data from PDB files, saving molecular coordinates in PDB

format 3

Total hours 30

TEACHING TOOLS USED

N1 Demonstration

1

0

N2 Tutored practical assignments

N3 Individual practical assignments

N4 Using common software for problem solving


Evaluation F – forming (during

semester),


semester end)

Educational effect

number

Way of evaluating educational effect

achievement

F1 PEK_U01 Individual tasks – finding specified

sequences and structures in databases (max.

2 points)

F2 PEK_W01,

PEK_U02

Individual tasks – an algorithm solving a

simple problem (max 2 points)

F3 PEK_W02,

PEK_U02

Individual tasks on coding with control

statements (max. 3 points)

F4 PEK_U02 Individual tasks – biological sequence data

processing (max 6 points)

F5 PEK_W03,

PEK_W04,

PEK_U02,

PEK_U03

Individual tasks: programs processing

biological sequences read and written using

FASTA formatted files

F6 PEK_W03,

PEK_W04,

PEK_U04

Individual tasks: programs parsing data

from PDB files and saving molecular

coordinates in PDB format

C = 3.0 if (F1+F2+F3+F4+F5+F6)=14-16,5 points

3.5 if (F1+F2+F3+F4+F5+F6)=17-19,5 points

4.0 if (F1+F2+F3+F4+F5+F6)=20-22,5 points

4.5 if (F1+F2+F3+F4+F5+F6)=23-25,5 points

5.0 if (F1+F2+F3+F4+F5+F6)=26-28 points

5.5 if (F1+F2+F3+F4+F5+F6)=26-28 points, and at least in one of coded programs

employed are syntax or tools not covered on classes. Examples: object oriented

programming, exceptions, GUI, Biopython)

1

1


PRIMARY LITERATURE:

[1] Any basic book on python, e.g. „Python – introduction” by Lutz Mark, or

[2] online python documentation: http://www.python.org/doc/


[1] Entrez Sequences Help: https://www.ncbi.nlm.nih.gov/books/NBK44864/

[2] PDB File format: http://www.pdb.org/pdb/static.do?p=file_formats/index.jsp#pdb

[3] Biopython documentation:

http://www.pdb.org/pdb/static.do?p=file_formats/index.jsp#pdb

SUBJECT SUPERVISOR (NAME AND SURNAME, E-MAIL ADDRESS)

Paweł Kędzierski, Ph.D., [email protected]


FOR SUBJECT

Basics of bioinformatics


Biotechnology

Subject

educational

effect





Subject

objectives***

Programme

content***

Teaching tool

number***

(knowledge)

PEK_W01 T1A_U07, T1A_U10, InzA_U03 C1 La1-La4 N1-N4


PEK_W03 T1A_U07, T1A_U10, InzA_U03 C2 La8 N1-N4


(skills)PEK_U

01 T1A_U07, T1A_U10, InzA_U03 C2 La8 N1-N4

PEK_U02 T1A_U07, T1A_U10, InzA_U03 C1, C3 La1-La5 N1-N4

PEK_U03 T1A_U07, T1A_U10, InzA_U03 C3 La9 N1-N4

PEK_U04 T1A_U07, T1A_U10, InzA_U03 C3 La10 N1-N4



mailto:[email protected]

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Zał. nr 4 do ZW 64/2012

FACULTY CHEMISTRY / DEPARTMENT Biochemistry

SUBJECT CARD

Name in Polish Biochemia

Name in English Biochemistry Main field of study (if applicable):Erasmus students

Level and form of studies: 1st

Kind of subject: obligatory


Group of courses NO


Number of hours of


University (ZZU)

60


student workload

(CNPS)

90

Form of crediting Examination /

crediting with

grade*

Examination /

crediting with

grade*

crediting with

grade Examination /

crediting with

grade*

Examination /

crediting with

grade*

For group of courses

mark (X) final course


points for practical (P)

classes

3



student contact (BK)

classes

2


PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES

Basic knowledge of chemistry, biology and biochemistry \

SUBJECT OBJECTIVES C1. Introduction to basic techniques of working with biomolecules C2. The basic skills for determining parameters describing the kinetics of enzymatic reactions


relating to skills:

A person who has completed the course: PEK_U01 - can determine the concentration of protein (Lowry method, Bradford method, A280 measure) PEK_U02 - knows how to assess the nature of inhibition of enzymatic reaction (competitive inhibitor - non-competitive inhibitor – uncompetitive inhibitor) PEK_U03 - can perform chromatographic separation of proteins, gel filtration technique; choose the right gel; determine the void volume, and Kav

PEK_U04 - can perform protein electrophoresis with SDS-PAGE PEK_U05 - knows how to isolate DNA from animal tissue, and how determine the purity of the product, melting point and the degree of renaturation

1

3

PEK_U06 - can determine basic properties of the protein: pI, molecular weight, optimum pH and temperature, the amount of sulfhydryl and disulfide bridges

Form of classes - laboratory Number of

hours

Lab 1 Introductory info, safety rules, pipetting, spectrophotometry 4

Lab 2 Enzyme kinetics I 4

Lab 3 Enzyme kinetics II 4

Lab 4 4 Ellman method – protein thiols determining 4

Lab 5 5 Peptide disulfide bridges determining 4

Lab 6 Enymatic hedrolysis 4

Lab 7 Gel filtration 4

Lab 8 Effect of temperature on enzyme activity 4

Lab 9 Effect of pH on enzyme activity 4

Lab 10 DNA preparation 4

Lab 11 Amino acid and protein pH titration 4

Lab 12 Proteins SDS-PAGE electrophoresis 4

Lab 13 Widma różnicowe białek 4

Lab 14 Krzywa topienia DNA 4

Lab 15 Kolokwium, termin odróbkowy 4

Total hours 60

TEACHING TOOLS USED

N1. Theoretical introduction

N2. Practical approach


Evaluation (F – forming

(during semester), P –

concluding (at semester

end)

Educational effect

number Way of evaluating educational effect achievement

F1 Final test

F2 Exercise report

P (test) = 3,0 jeżeli (F1+F2) = 60,0 – 70,0 pts

3,5 if (F1+F2) = 70,1 – 75,0 pts

4,0 if (F1+F2) = 75,1 – 80,0 pts

4,5 if (F1+F2) = 80,1 – 85,0 pts

5,0 if (F1+F2) = 85,1 – 90,0 pts

5,5 if (F1+F2) = 90,1 – 100,0 pts


1

4

PRIMARY LITERATURE:

[1] 1. Berg, J.M., Tymoczko, J.L., Stryer, L. „Biochemistry” W.H. Freeman and Co., New

York – 7th

edition 2012

[2] Berg, J.M., Tymoczko, J.L., Stryer, L. „Biochemia” PWN SA 2005/6 (6-th polish edition)

[3] Instructions for laboratory classes (network-accessible).


[1] Voet, D., Voet, J.G. „Biochemistry” Wiley & Sons, Inc., 3rd

edition


Piotr Dobryszycki; [email protected]

1

5

MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR

SUBJECT

BIOCHEMISTRY


Biotechnology

Subject educational

effect Correlation between subject

educational effect and

educational effects defined for

main field of study and

specialization (if applicable)**

Subject

objectives*** Programme content*** Teaching tool

number***

PEK_U01 (skills) K1Abt_U20 C1 Lab1,Lab5, La13, Lab14 N1, N2

PEK_U02 K1Abt_U20 C2 Lab2, Lab3, Lab6 N1, N2

PEK_U03 K1Abt_U20 C1 Lab7 N1, N2

PEK_U04 K1Abt_U20 C1 Lab12 N1, N2

PEK_U05 K1Abt_U20 C1 Lab10, Lab14 N1, N2

PEK_U06 K1Abt_U20 C1

Lab4, Lab5, Lab8, Lab9,

Lab11 N1, N2



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6

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Inżynieria Chemiczna

Name in English Chemical Engineering Main field of study (if applicable) Chemical Technology




Subject code ICC013009

Group of courses NO *delete as applicable


Number of hours of


University (ZZU) 30




with grade


(X) final course

Number of ECTS points 2








COMPETENCES

6. Completion physics

7. Completion mathematics

SUBJECT OBJECTIVES

C1 Introduce with chemical and physical basis of basic chemical engineering processes

C2 Cognition of form rules of heat and mass balances in the steady state and unsteady

state conditions.

C3 Cognition of mathematical modeling and design rules of processes and apparatus

used in chemical engineering and processing

C4 Cognition of scale-up rules

C5 Usage of hydrostatics and hydrodynamics rules for description of apparatus occur in

industrial installations

C6 Cognition of rules choice of pumps and other flow apparatus

C7 Cognition of rules of apparatus calculation with two phases flow

C8 Cognition of mathematical methods of heat exchangers description and design

C9 Introduction to balancing and operation parameters calculation for selected mass

1

7

transfer apparatus

C10 Carrying out of pressure drops measurements in order to determine flow velocity.

C11 Carrying out of stream volume measurement

C12 Experimental determining of heat and mass transfer coefficients

C13 Experimental determining of reflux ratio in rectification column and graphical

interpretation of column operation



PEK_W01 – Know chemical and physical basis of selected processes and oparations occur

in chemical engineering

PEK_W02 – Can define heat and mass balances in steady state and unsteady state

conditions.

PEK_W03 – Can describe with the use of mathematical model and design selected processes

and apparatus used in chemical engineering

PEK_W04 – Know rules of scale-up

Relating to skills:

PEK_U01 – Can describe apparatus operation used in industrial plants using rules of

hydrostatics and hydrodynamics

PEK_U02 – Can choice pumps and other apparatus cooperating with pipeline

PEK_U03 – Can calculate heat exchangers area and determine heat exchanger operation

parameter

PEK_U04 – Can form mass balances and determine operation parameters of selected mass

exchangers

PEK_U05 – Can use appropriate metering equipment for determination of pressure drop and

can calculate fluid flow velocity

PEK_U06 – Can carry out of volume stream of gas or liquid

PEK_U07 – Can experimentally measure heat and mass transfer coefficients

PEK_U08 – Can experimentally determine reflux ratio and use to calculation of operating

lines of rectification process


Lab 1 Organizational activities. Becoming acquainted with rules of health

and safety at work in research laboratory. Discuss to meet the

completion requirements. Take knowledge of apparatus used in

laboratory.

3

Lab 2 Determination of fluid flow profile in the pipeline with circular cross

– section.

3

Lab 3 Pump characteristics. 3 Lab 4 Determination of flow coefficient in flow narrow for liquids. 3

Lab 5 Heat exchanger pipe in pipe type. 3 Lab 6 Heat transfer during liquid boiling 3 Lab 7 Efficiency of mixing energy on the mass transfer coefficient in the

solid – liquid system.

3

Lab 8 Determination of HETP in packed bed rectification column. 3 Lab 9 Distillation with the steam. 3

Lab 10 Heat transfer in fluidized bed. 3

1

8

Total hours 30

TEACHING TOOLS USED

N1 Informational lecture

N2 Multimedia presentation

N3 Solution of problems

N4 Application of Excel for specialist calculations.

N5 Realization of experiments.

N6 Report description.


Evaluation


semester),


semester end)

Educational effect


achievement

C(lecture) PEK_W01 –

PEK_W04

Exam

F1 PEK_U01 –

PEK_U02

Verification colloquium I – class

F2 PEK_U03 -

PEK_U04

Verification colloquium II – class

Cl(ćwiczenia) = (F1+F2)/2

F3 PEK_U05 –

PEK_U08

Appraise a student's reports and colloquium

after each laboratory exercise.

C (laboratory) = mean of reports and colloquium marks


PRIMARY LITERATURE:

[1] J. Ciborowski, Podstawy inżynierii chemicznej, WNT, Warszawa1982 [2] M. Serwiński, Zasady inżynierii chemicznej i procesowej, WNT, Warszawa 1982 [3] Koch Roman, Noworyta Andrzej: Procesy mechaniczne w inżynierii chemicznej.

Warszawa : WNT, 1992.

[4] Koch Roman, Kozioł Antoni: Dyfuzyjno-cieplny rozdział substancji. Warszawa : WNT,

1994.

[5] Zadania rachunkowe z inżynierii chemicznej, (pr. zbiorowa pod red. R.Zarzyckiego),

PWN W-wa 1980. [6] Z. Kawala, A. Kołek, M. Pająk, J. Szust, Zbiór zadań z podstawowych procesów

inżynierii chemicznej cz. I – III. Skrypty PWr.

[7] Laboratorium Inżynierii Procesowej cz.I. Przenoszenie pędu i procesy mechaniczne

oraz cz.II. Przenoszenie ciepła i masy – praca zbiorowa pod redakcją Danuty Beliny-

Freundlich, Wrocław 1981.

[8] [2] Instrukcje do ćwiczeń, dostępne na stronie Wydziału Chemicznego PWr.


[4] K.F.Pawłow, P.G.Romankow, A.A.Noskow. Przykłady i zadania z zakresu aparatury i

1

9

inżynierii chemicznej, WNT W-wa 1988

[5] Selecki A., Gradoń L., Podstawowe procesy przemysłu chemicznego, WNT, Warszawa1985. [6] Kembłowski Z., Podstawy teoretyczne inżynierii chemicznej i procesowej, WNT, Warszawa

1985 [7] Hobler T., Ruch ciepła i wymienniki, WNT, Warszawa1986.

SUBJECT SUPERVISOR

(NAME AND SURNAME, E-MAIL ADDRESS)

Dr inż. Wojciech Skrzypiński, [email protected]


FOR SUBJECT

Chemical Engineering


Chemical Technology

Subject

educational

effect





Subject



number***

(knowledge)

PEK_W01

(knowledge)

PEK_W01 K1Atc_W12 C1 Wy1 N1, N2

PEK_W02 K1Atc_W12 C2, C3, C8,C9

Lec 1, Lec 5,

Lec 7, Lec 8,

Lec 15

N1, N2

PEK_W03 K1Atc_W12 C3, Lec 2 – Lec 15 N1, N2

PEK_W04 K1Atc_W12 C4 Lec 2 – Lec 15 N1, N2

(skills)

PEK_U01 K1Atc_U09 C5

Cl 1 – Cl 4,

Cl 7 – Cl 9 N3, N4

PEK_U02 K1Atc_U09 C6, C7 Cl 5, N3, N4

PEK_U03 K1Atc_U09 C8 Cl 10, Cl 11 N3, N4

PEK_U04 K1Atc_U09 C9 Cl 4, Cl 5,

Cl 7 – Cl 14 N3, N4

PEK_U05 K1Atc_U14 C10 Lab2, Lab4 N5, N6

PEK_U06 K1Atc_U14 C11 Lab2, - Lab5,

Lab7, - Lab10 N5, N6

PEK_U07 K1Atc_U14 C12 Lab5, - Lab7,

Lab10 N5, N6

PEK_U08 K1Atc_U14 C13 Lab8 N5, N6

Zał. nr 4 do ZW 64/2012


2

0



SUBJECT CARD

Name in Polish Procesy dyfuzyjne

Name in English Diffusion Processes Main field of study (if applicable) Chemical and Process Engineering

Specialization (if applicable)






Number of hours of


University (ZZU) 45 45 30


student workload (CNPS) 120 90 60

Form of crediting Examination Examination

/ crediting

with grade*

Crediting

with grade Crediting

with grade Examination

/ crediting

with grade* For group of courses mark

(X) final course

Number of ECTS points 4 3 2 including number of ECTS

points for practical (P) classes 3 2



student contact (BK) classes 2 1,5 1



COMPETENCES

8. Know of physical chemistry and processes thermodynamic

9. Know of foundations of chemical engineering

SUBJECT OBJECTIVES

C1 Introduce of theory of mass transfer between two phases.

C2 Classification methods of mass transfer apparatus.

C3 Know mathematical description of mass transfer rate in both diffusional and thermo-

diffusional processes.

C4 Introduce of calculation methods of selected apparatus used for diffusional and

thermo-diffusional separation of components.

C5 Learn carrying out simple calculations of kinetic parameters of mass transfer

processes.

C6 Learn to work out project procedures of selected mass transfer apparatus.

C7 Introduce of selected measurements methods of characteristic parameters of mass

transfer processes in different apparatus.

2

1



PEK_W01 – know theory of mass transfer processes

PEK_W02 – can classificate of mass transfer apparatus.

PEK_W03 – know mathematical description of diffusional and thermo-diffusional mass

transport.

PEK_W04 – know methods of description mass transfer processes occurring in the different

construction mass transfer apparatus

Relating to skills:

PEK_U01 – can match mass transfer apparatus for realization of different mass transfer

processes.

PEK_U02 – can carry out balance and kinetic calculations different kinds of mass transfer

apparatus.

PEK_U03 – can make experimental measurements of characteristic parameters of mass

transfer in laboratory scale apparatus.

PROGRAMME CONTENT


Lec 1 Theory of diffusion in gas and liquid phases, diffusivity fo two- and

multicomponent mixtures, equation of diffusion rate. 3

Lec 2 Mass transfer and overall mass transfer processes, expression

methods of mass transfer and overall mass transfer coefficients. 3

Lec 3 Classification of mass transfer apparatus, number of theoretical

stages. 3

Lec 4 Number of real stages, definitions of stage efficiency. 3

Lec 5 Colburn method. 3

Lec 6 Absorbers, rules of realization and design of absorption process. 3

Lec 7 Distillation equilibria, examples of simple distillations, steady state

and unsteady state processes. 3

Lec 8 Rectification of two component mixtures, minimal number of

theoretical plates (stages), minimal reflux ratio. 3

Lec 9 Multicomponent rectification, rules of design. 3

Lec 10 Special cases of rectification, column and systems for azeptropes

separation, using of separating components. 3

Lec 11 Extractors, methods of process realization, process design using

Gibbs triangle and Cartesian diagram. 3

Lec 12 Extractors design, drop diameter, flooding, Thornton equation,

calculation of mass transfer coefficients and overall mass transfer

coefficients, calculation of column diameter and column high.

3

Lec 13 Adsorbers design, methods of realization of adsorption process. 3

Lec 14 Drying processes, description of moist air, Molier diagram, dryers

design. 3

Lec 15 Using of new method of separation, membrane processes,

perspectives of chemical engineering developments. 3

Total hours 45

2

2


Lab1 Organizational activities. Becoming acquainted with rules of health

and safety at work in research laboratory. Presentation of basic

apparatus used in experiments.

2

Lab2 Extraction efficiency in the liquid - liquid system. 2 Lab3 Volume overall mass transfer coefficient and high of mass transfer

unit.

2

Lab4 Influence of mixing energy on mass transfer coefficient in the solid –

liquid system.

2

Lab5 Influence of mixing energy on mass transfer in RDC column. 2 Lab6 Efficiency of sieve plate in the desorption process of gas. 2 Lab7 Extraction efficiency in the liquid - liquid system II. 2 Lab8 Partial colloquium I. 2 Lab9 Influence of liquid pulsation on mass transfer rate. 2 Lab10 Volume overall mass transfer coefficient and high of mass transfer

unit.II.

2

Lab11 Mass transfer from solid surface in conditions of natural convection. 2 Lab12 Determination of mass transfer coefficient from solid surface in

conditions forced convection.

2

Lab13 Measurement of axial mixing with the use of impulse method. 2 Lab14 Supplementary laboratory, partial colloquium II. 2 Lab15 Repeat colloquium and credit. 2 Total hours 30

Form of classes - project Number of hours

Proj 1 Calculation methods of overall mass transfer coefficients in the gas

– liquid systems. Project I – absorber for elimination of CO2 from air

with use of water. Partial colloquium I.

15

Proj 2 Balance calculations of simple distillations and rectifications in two

component system. . Project II – apparatus for equilibrium and batch

distillation and for rectification in the system acetic acid – water.

Partial colloquium II.

18

Proj 3 Methods of realization and calculation of liquid – liquid extraction

processes. Project III – Comparison of multistage cross flow and

countercurrent flow processes. Partial colloquium III.

12

Total hours 45

TEACHING TOOLS USED

N1 Lecture with multimedia instruments.

N2 Solving of a problems.

N3 Implementation of calculations and design with using own procedures worken out in

Excel.

N4 Presentation of project.

N5 Experiments performance and preparing of report.

2

3


Evaluation


semester),


semester end)

Educational effect


achievement

C(lecture) PEK_W01 –

PEK_W04

Examination

F1(project) PEK_U01,

PEK_U02

Partial colloquium I

F2(project) PEK_U01,

PEK_U02

Project report I

F3(project) PEK_U01

PEK_U02

Partial colloquium II,

F4(project) PEK_U01

PEK_U02

Project report II

F5(project) PEK_U01

PEK_U02

Partial colloquium III,

F6(project) PEK_U01

PEK_U02

Project report III

C(project) = (F1+0,8F2+F3+0,8F4+F5+0,8F6)/6

F1 (laboratory) PEK_U03 Partial colloquium I

F2 (laboratory) PEK_U03 Partial colloquium II

F3 (laboratory) PEK_U03 Evaluate of reports La2 – La7, La9 – La13

and calculation of average grade

C(laboratorium) = (F1+F2+F3)/3


PRIMARY LITERATURE:

[9] Z. Ziołkowski, Destylacja i rektyfikacja w przemyśle chemicznym, WNT Warszawa

1978.

[10] J. Ciborowski, Podstawy inżynierii chemicznej, WNT, Warszawa1982. [11] M. Serwiński, Zasady inżynierii chemicznej i procesowej, WNT, Warszawa 1982.

[12] Koch Roman, Noworyta Andrzej: Procesy mechaniczne w inżynierii chemicznej.

Warszawa : WNT, 1992.

[13] Koch Roman, Kozioł Antoni: Dyfuzyjno-cieplny rozdział substancji. Warszawa : WNT,

1994.

[14] Zadania rachunkowe z inżynierii chemicznej, (pr. zbiorowa pod red. R.Zarzyckiego),

PWN W-wa 1980. [15] Z. Kawala, A. Kołek, M. Pająk, J. Szust, Zbiór zadań z podstawowych procesów

inżynierii chemicznej cz. I – III. Skrypty PWr.

[16] Praca zbiorowa, Zadania projektowe z inżynierii procesowej, Oficyna Wydawnicza

Politechniki Warszawskiej, W-wa 1986.

[17] Laboratorium Inżynierii Procesowej cz.I. Przenoszenie pędu i procesy mechaniczne

oraz cz.II. Przenoszenie ciepła i masy – praca zbiorowa pod redakcją Danuty Beliny-

Freundlich, Wrocław 1981.

[18] Instrukcje do ćwiczeń, dostępne na stronie Wydziału Chemicznego PWr.

2

4


[8] Don Green, Robert Perry. Perry's Chemical Engineers' Handbook, Eighth Edition,

McGraw-Hill Professional; 8 edition (November 13, 2007). [9] R. Byron, Warren E. Stewart, Edwin N. Lightfoot. Transport Phenomena, Revised 2nd

Edition. John Wiley & Sons, Inc.; 2nd edition (December 11, 2006).

[10] E. L. Cussler. Diffusion: Mass Transfer in Fluid Systems (Cambridge Series in

Chemical Engineering), Cambridge University Press; 3 edition (February 2, 2009).

[11] K.F.Pawłow, P.G.Romankow, A.A.Noskow. Przykłady i zadania z zakresu aparatury i

inżynierii chemicznej, WNT W-wa 1988.

[12] Selecki A., Gradoń L., Podstawowe procesy przemysłu chemicznego, WNT, Warszawa1985. [13] Kembłowski Z., Podstawy teoretyczne inżynierii chemicznej i procesowej, WNT, Warszawa

1985.

SUBJECT SUPERVISOR


Dr inż. Roman Szafran, [email protected]


FOR SUBJECT

Diffusion Processes


Chemical and Process Engineering

Subject

educational

effect





Subject



number***

(knowledge)

PEK_W01 K1Aic_W24 C1 Lec1, Lec 2 N1

PEK_W02 K1Aic_W24 C2 Lec 3 N1

PEK_W03 K1Aic_W24 C3 Lec 4, Lec 5 –

Lec 15 N1

PEK_W04 K1Aic_W24 C4 Lec 5 – Lec 15 N1

(skills)

PEK_U01 K1Aic_U22 C4, C5 Pr1 – Pr3 N2 – N4

PEK_U02 K1Aic_U22 C5, C6 Pr1 – Pr3 N2 – N4

PEK_U03 K1Aic_U22 C7 La1 – La15 N5



2

5

Zał. nr 4 do ZW 64/2012

FACULTY Chemistry / DEPARTMENT Biochemistry

SUBJECT CARD

Name in Polish Enzymologia

Name in English Enzymology Main field of study (if applicable): Erasmus students

Level and form of studies: 1st


Subject code BTC l

Group of courses NO


Number of hours of organized classes in University

(ZZU)

45

Number of hours of total student workload (CNPS) 180

Form of crediting crediting with

grade

For group of courses mark (X) final course Number of ECTS points 3 including number of ECTS points for practical (P) classes 3

including number of ECTS points for direct teacher-

student contact (BK) classes 1.5



Basic biology and chemistry courses

\

SUBJECT OBJECTIVES C1 to acquaint students with the practical aspects of working with enzymes (isolation,

purification to homogeneity, the initial molecular characterization – N-terminus DNS labeling);

-C end digestion kinetics with CPA enzyme)

C2 familiarization with the techniques used in enzymology (centrifugation, protein salting,

spectrophotometric determination of protein concentration and enzyme – FDP aldolase

activity)

C3 determination of the phosphate content in biological material

C4 isolation and purification rabbit muscle aldolase A


relating to knowledge:

Student:

PEK_W01 - knows the basic methods of enzymology

PEK_W02 - has knowledge of the techniques of isolation, purification, and description

of the enzymes

PEK_W03 - has knowledge of how to determine the concentration of proteins and of

enzymatic activity

relating to skills:

Student:

PEK_U01 - is able to determine the protein concentration by the Bradford method and

using the Beer-Lambert law by measuring A280)

2

6

PEK_U02 - can determine the enzyme specific and total activity

PEK_U03 - is able to obtain a homogeneous enzyme from biological material

PEK_U04 – can label the the N-terminal end of protein with dansyl chloride

PEK_U05 - is able to balance the enzyme preparation (yield and purity of enzyme

preparation)

PEK_U06 - is able to determine the content of phosphate in biological materials

PROGRAMME CONTENT


hours

Lab 1 Intro; lab safety rules; laboratory equipment (spectrophotometer, centrifuge,

pH-meter, fraction collector, thermoblock, etc.); theory of FDP-aldolase

action, actvity and protein concetration calculation and measurements

6

Lab 2 Protein concentration measurements; Bradford method; analysis of the effect

of surfactant, denaturant, salt on concentration measure. Determination of

phosphate content in the biological samples with the Ames method.

6

Lab 3 Aldolase activity measurements with the hydrazine method – aldolase

activity, specific activity, total activity; preparation summary. Comparison

hydrazine test with the enzymatic test. Preparation of ammonium sulphate.

6

Lab 4 Rabbit muscle aldolase A isolation and purification with the Taylor method. 6

Lab 5 Peptide N-terminal residue determination – dansyl method. 6

Lab 6 Peptide N-terminal residue identification - TLC chromatography after dansyl

labeling and acid hydrolysis. 6

Lab 7 Analysis of the effect of carboxypeptidase A digestion on the aldolase activity 6

Lab 8 Final test. 3

Total hours 45

TEACHING TOOLS USED

N1 introduction to the experiment





end)

Educational effect


P (laboratorium) PEK_W01 –

PEK_W08

crediting with grade


2

7

PRIMARY LITERATURE:

[1] Laboratory instructions for excercises (placed on the faculty e-portal).

[2] Set of the original papers (placed on the faculty e-portal)


[1] Berg, J.M., Tymoczko, J.L., Stryer, L. „Biochemistry” W.H. Freeman and Co., New York –

7th

edition 2012

[2] Berg, J.M., Tymoczko, J.L., Stryer, L. „Biochemia” PWN SA 2009 (tłumaczenie 6 wydania

amerykańskiego)


edition.


Piotr Dobryszycki, PhD, DSc [email protected]

2

8


SUBJECT

ENZYMOLOGY


Biotechnology

Subject educational effect Correlation between subject





Subject

objectives*** Programme content*** Teaching tool

number***

(knowledge)

PEK_W01 K1Abt_U25 C1, C2 La1, La4, La5, La8 N1

PEK_W02 K1Abt_U25 C2 La2, La4, La5-La8 N1

PEK_W03 K1Abt_U25 C1-C3 La1, La2, La4, La5,

La8 N1

(skills)

PEK_U01 K1Abt_U25 C1 La1, La2 N1

PEK_U02 K1Abt_U25 C1 La4, La5, La8 N1

PEK_U03 K1Abt_U25 C1, C2, C4 La5 N1

PEK_U04 K1Abt_U25 C1, C2 La6, La7 N1

PEK_U05 K1Abt_U25 C1, C4 La5 N1

PEK_U06 K1Abt_U25 C3 La3 N1



2

9

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Podstawy inżynierii chemicznej

Name in English Foundations of Chemical Engineering Main field of study (if applicable) All fields of Faculty of Chemistry





Group of courses YES *delete as applicable


Number of hours of


University (ZZU) 30



Form of crediting crediting

with grade

Examination

/ crediting

with grade*

Examination

/ crediting

with grade*

Examination

/ crediting

with grade*

Examination

/ crediting


(X) final course









COMPETENCES

10. Knowledge of physics and mathematics on the high school (secondary school) level

SUBJECT OBJECTIVES

C1 Cognition of quantitative description of fluid flow processes in apparatas including

drops pressure.

C2 Using of Bernoulli law for quantitative description of metering equipments and heat

and mass transfer apparatus.

C3 Specify of heat transfer methods.

C4 Specify of interphase mass transfer.

C5 Cognition of construction rules and operation of selected industrial equipment and

apparatus.

3

0



PEK_W01 – Know different types of flows in industrial flowing equipment and apparatus

used for heat and mass transfer.

PEK_W02 – Know Bernoulli law and its application for description of different types of

flows in the equipment and apparatus.

PEK_W03 – Know methods of heat transfer in the heat-exchangers.

PEK_W04 – Distinguish mass transfer and overall mass transfer and is able to describe mass

transfer rate of components.

PEK_W05 – Know cognition of construction rules and influence of operating parameters on

the processes in selected apparatus: pumps, sedimentators, filters, separators of

dusts, mixers, chemical reactors, and distillation, absorption, extraction,

adsorption, drying apparatus.

PROGRAMME CONTENT


Lec 1 Interest area of chemical engineering and basic values used for

processes description. 2

Lec 2 Balancing rules streams and apparatus. 2

Lec 3 Fluid flow in apparatus, Bernoulli equation, pressure drops in

pipeline and in selected apparatus. 2

Lec 4 Pumps – characteristics of pump and pipeline. Calculation of work

point in selected configurations pump – pipeline. 2

Lec 5

Motion of particles in the fluids. Calculation of particle diameter,

calculation of motion velocity, fall of particles set, fluidization,

pneumatic transport, sedimentation.

2

Lec 6 Filtration. Filter construction, classification of filtration processes,

used filters in selected technologies. 2

Lec 7 Mixers, construction of stirrers and mixers, consumption of energy. 2

Lec 8 Heat transfer processes and heat exchangers. 2

Lec 10 Absorption processes. Absorption apparatus, methods of description

mass transfer process, methods of realization absorption process. 2

Lec 11

Distillation processes. Equilibrium distillation, batch distillation,

distillation with the steam, thin layer distillation, molecular

distillation. Rules of balancing.

2

Lec 12 Rectification of two-component systems. Construction of

rectification column, heat and mass balances of process. 2

Lec 13

Extraction apparatus. Periodic apparatus and continuous apparatus.

Calculation methods with using Gibbs triangle. Calculation of the

extraction column diameter and column high by means of selected

methods.

2

Lec 14 Drying processes. Drying medium – Molier diagram. Construction of

dryers, time of drying. 2

Lec 15 Credits colloquium 2

Total hours 30

3

1

TEACHING TOOLS USED

N1 Informational lecture



Evaluation


semester),


semester end)

Educational effect


achievement

C (lecture) PEK_W01 –

PEK_W05 Colloquium


PRIMERY LITERATURE:

[19] Koch R., Noworyta A.: Procesy mechaniczne w inżynierii chemicznej. Warszawa :

WNT, 1992.

[20] Koch R., Kozioł A.: Dyfuzyjno-cieplny rozdział substancji. Warszawa : WNT, 1994.

[21] Ciborowski J., Podstawy inżynierii chemicznej, WNT, Warszawa1982 [22] Serwiński M., Zasady inżynierii chemicznej i procesowej, WNT, Warszawa 1982 [23] Selecki A., Gradoń L., Podstawowe procesy przemysłu chemicznego, WNT, Warszawa1985.


[14] Kembłowski Z., Podstawy teoretyczne inżynierii chemicznej i procesowej, WNT, Warszawa

1985.

[15] Hobler T., Ruch ciepła i wymienniki, WNT, Warszawa1986.

SUBJECT SUPERVISOR


Prof. dr hab. inż. Andrzej Matynia, [email protected]

Prof. dr hab. inż. Andrzej Noworyta, [email protected]

Dr inż. Wojciech Skrzypiński, [email protected]




3

2


FOR SUBJECT

Foundations of Chemical Engineering


All fields of Faculty of Chemistry

Subject

educational

effect





Subject



number***

(wiedza)

PEK_W01

K1Abt_W09, K1Ach_W10,

K1Aic_W09, K1Atc_W09,

K1Aim_W09

C1 Lec1 – Lec7 N1, N2

PEK_W02



K1Aim_W09

C2 Lec3 N1, N2

PEK_W03



K1Aim_W09

C3 Lec8 N1, N2

PEK_W04



K1Aim_W09

C4 Lec10 – Lec14 N1, N2

PEK_W05



K1Aim_W09

C5 Lec10 – Lec14 N1, N2



3

3

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Podstawy chemii analitycznej

Name in English Fundamentals in analytical chemistry Main field of study (if applicable)

All fields


Level and form of studies: 1st/ 2nd* level, full-time / part-time*

Kind of subject obligatory / optional / university-wide*

Subject code CHC014011

Group of courses YES / NO* *delete as applicable


Number of hours of


University (ZZU) 30




with grade*


(X) final course








COMPETENCES

11. Has a general knowledge in general chemistry

12. Has a general knowledge in inorganic chemistry

SUBJECT OBJECTIVES

C1 Introduction to basic concepts and methods of the analytical chemistry

C2 Getting to know with the analytical procedure, aimed at the determination or the

detection of components in analyzed samples, and its stages

C3 Getting to know with methods of the sampling and the sample preparation of

samples prior to measurements

C4 Getting to know with the laboratory practice in the field of classical methods of the

quantitative chemical analysis (gravimetric and volumetric methods of the analysis)

3

4



The person who passed the course

PEK_W01 – knows basic concepts and methods of the analytical chemistry

PEK_W02 – knows principles of the analytical procedure aimed at the determination or the

detection of specific components of analyzed samples

PEK_W03 – knows methods of the sampling of different batches of samples and the

preparation of laboratory and analytical samples

PEK_W04 – knows methods of the wet digestion in open- and closed-vessel systems, the

dry ashing and the fusion with fluxes

PEK_W05 – knows methods of the separation of components in samples, i.e., the

precipitation, extraction and chromatographic methods

PEK_W06 – knows theoretical and practical applications of gravimetric and volumetric

methods of the analysis

PEK_W07 – knows the statistical treatment of results of the analysis (measures of the

location and the dispersion of measurement series, types of errors)

Relating to skills:

The person who passed the course

PEK_U01 – correctly performs various elementary operations of the classical chemical

analysis (the weighing, the precipitation, the filtration, the sampling, the

titration)

PEK_U02 – is able to perform simple quantitative determinations using gravimetric,

volumetric and spectrophotometric methods of the analysis

PEK_U03 – is able to describe the course of the analysis for by chemical reactions

PEK_U04 – is able to calculate results of the analysis

Form of classes – laboratory Number of hours

Lab 1 Guidelines for the safe working in a chemistry lab. How to

conduct and pass the course 2

Lab 2 –

Lab 3 The acidimetric determination of HCl in a solution (setting the

HCl concentration for sodium carbonate) 4

Lab 4 –

Lab 5 A short test. The determination of Na2CO3 and NaOH in a

solution (acid-base titration with HCl) 4

Lab 6 –

Lab 7 A short test. The determination of Fe and Ni in a solution (1) –

the gravimetric analysis of iron after the separation of nickel 4

Lab 8 –

Lab 9

The determination of Fe and Ni in a solution (2) – the

gravimetric analysis of iron (cont.). The volumetric

determination of the sum of Fe and Ni

4

Lab 10 –

Lab 11

A short test. The determination of Fe and Ni in a solution (3) –

the determination of Fe by a red-ox titration 4

Lab 12 –

Lab 13

The chemical analysis of water (1) – the determination of the

water hardness, the determination of the content of chloride ions 4

Lab 14 –

Lab 15

A short test. The chemical analysis of water (2) – the determination of the

dissolved oxygen content, the ammonia nitrogen determination 4

Total hours 30

3

5

TEACHING TOOLS USED

N1 Informative lectures

N2 Problem lectures

N3 Implementation of quantitative analytical determinations

N4 Preparation of reports

N5 Consultations


Evaluation


semester),


semester end)

Educational effect


achievement

C (lecture) PEK_W01-

PEK_W08

Final examination

F1 (laboratory) PEK_U01-

PEK_U04

Arithmetic mean of marks for analyses

conducted (8 overall)

F2 (laboratory) PEK_U02-

PEK_U04

Short tests 1-4 (maximally 12 points)

F2 = 3.5 if 6-7.5 points

4.0 if 7.75-9.0 points

4.5 if 9.25-10.5 points

5.0 if 10.75-12.0 points


PRIMARY LITERATURE:

[1] A. Cygański, Chemiczne metody analizy ilościowej. Wyd. 5. WNT Warszawa, 1999

[2] J. Minczewski, Z. Marczenko, Chemia analityczna t. I i II, PWN Warszawa, 2001

[3] T. Lipiec, Z.S. Szmal, Chemia analityczna z elementami analizy instrumentalnej, Wyd.

7. PZWL Warszawa, 1996

[4] D.A. Skoog, D.M. West, F.J. Holler, S.R. Crouch, Podstawy chemii analitycznej.

Przekład z ang. WN PWN Warszawa, 2006


[1] Ćwiczenia rachunkowe z chemii analitycznej. Praca zbiorowa pod red. Z. Galusa, PWN

Warszawa, 1993

SUBJECT SUPERVISOR


Dr hab. inż. Paweł Pohl, Prof. PWr, [email protected]


3

6


FOR SUBJECT

…………………………………….


…………………………………….

Subject

educational

effect





Subject



number***

(knowledge)

PEK_W01 –

PEK_W08

K1Abt_W11, K1Aic_W11,

K1Aim_W11, K1Atc_W11,

K1Ach_W09

C1, C2, C3 Lec 1 – Lec 8 N1, N2

(skills)

PEK_U01 –

PEK U04

K1Abt_U19, K1Ach_U10,

K1Aic_U10, K1Aim_U11, K1Atc_U11 C4 Lab 2 – Lab 15 N3, N4, N5



3

7

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Podstawy technologii chemicznej

Name in English Fundamentals of chemical technology Main field of study (if applicable) lecture - all students of the Faculty of Chemistry

project-Chemistry, Chemical Technology,

Engineering material


Level and form of studies: 1st/ full-time /

Kind of subject obligatory /




Number of hours of


University (ZZU) 30 30


student workload (CNPS) 90 60


with grade crediting

with grade


(X) final course

Number of ECTS points 3 2 including number of ECTS




student contact (BK) classes 1 1



COMPETENCES

13. Knowledge of general chemistry: properties of substances, stoichiometry

14. Knowledge of physical chemistry: thermodynamics, kinetics

15. Knowledge of mathematics: differentiation, integration, differential equations

SUBJECT OBJECTIVES

C1 Getting to know with the basic concepts and laws in the field of chemical

technology.

C2 Getting to know with the material and thermal balance of the process.

C3 Getting to know with the physicochemical properties of substances and methods of

their evaluation.

C4 Getting to know with the engineering calculations of the chemical process.

C5 Teaching how to do simple projects using Spreadsheet and professional program

type of Chemcad and Polymath

3

8



PEK_W01 – knows the basic technological principles

PEK_W02 – knows the rules of preparing material and energy balance

PEK_W03 – knows the ways to predict the physicochemical properties of the substance

PEK_W04 – knows the basics of calculating the composition and temperature of the

reacting system

Relating to skills:

PEK_U01 – can reach for data sources with substance properties

PEK_U02 – is able to prepare simple material and energy balances and conduct their

analysis

PEK_U03 – can make simple engineering calculations

PEK_U04 – can make a quantitative block diagram diagram

PEK_U05 – can use a professional programs like Chemcad and Polymat

PROGRAMME CONTENT


Lec 1 Basic concepts: technological process, chemical method concept,

technological method concept. Discussion of technological

principles: the principle of the best use of potential differences, the

principle of the best use of raw materials, the principle of the best use

of energy, the principle of the best use of equipment, the principle of

technological moderation. Unit operations. Material balance of the

chemical process: the principle of mass conservation, the principle of

atomic behavior, the principle of energy conservation. Analysis of

material balance of steady-state processes.

2

Lec 2 Material balance of systems with chemical reaction. The degree of

conversion in the stoichiometric and non-stoichiometric mixture of

reagents. Process efficiency. Process diagram, stream diagram

simulation. Computer programs used to simulate chemical processes

(CHEMCAD

2

Lec 3 Energy balance. Basic concepts: layout, system state variables,

system state. The principle of energy conservation, energy

components of systems: internal energy, work, heat, enthalpy.

Calculation of enthalpy changes. Enthalpy of reaction. The influence

of temperature and pressure on the enthalpy of the reaction.

2

Lec 4 The ideal gas: the equation of the ideal gas state, properties.

Compressibility factor. Work of compression and expansion of gases.

Polytrop transformation. Balance sheets in a transient state.

Classification of chemical processes, balance types

2

Lec 5 Properties of chemical substances. Sources of technological

information - databases. Condensed phases. Prediction of

physicochemical properties: density, viscosity, critical parameters.

2

3

9

Thermodynamic properties. The method of group or atomic

increments, the method of states corresponding to each other. Critical

state of matter

Lec 6 Real gas. Deviations from the ideal state. Compression ratio for real

gases. Equations of real gas state. Acentric coefficient. Real gas

mixtures

2

Lec 7 Coefficient of gas and liquid activity. Definition of volatility and

volatility factor. Equations for the volatility factor calculation. The

volatility coefficient of the gas mixture component. Liquid activity

coefficient. Lewis-Randal's rule. Determination of activity

coefficients by means of group shares. Phase equilibria. The

functions of deviation from the ideal state

2

Lec 8 Chemical reaction. stoichiometry; concentration, concentration

relative to concentration and molar stream (change in volume). HSC

calculations. Direction of reaction; elimination of component

reactions as part of the chemical process concept. Composition

calculation (reaction run to the end).

2

Lec 9 Composition in balance. Constant balance. Temperature dependence

of the constant equilibrium. Reactions with a change in the number

of moles; pressure effect; technological treatments (excess reagent,

concentration reduction - examples). Calculation of the equilibrium

composition: ammonia synthesis, preparation of styrene, methane

conversion with water vapor.

2

Lec

10

Estimation of composition and temperature. Heat balance. Example:

hydrocarbon combustion, calculations assuming stoichiometry.

Example: preparation of sulfuric acid anhydride, stoichiometric and

equilibrium calculations. Assumption of adiabaticity.

2

Lec

11

Kinetic equation. The speed of the elementary reaction; concentration

dependence. Irreversible and reversible elementary reactions; solving

appropriate differential equations. Constant speed.

2

Lec

12

Variability of composition in time. Speed of real reaction; full kinetic

model, simplified descriptions. An approximation of the state of

equilibrium and an approximation of the stationary state. Examples

of complex reactions: decomposition of ozone, oxidation of nitric

oxide, combustion of hydrogen. Use of data: speed-degree of

conversion.

2

Lec

13

Tank reactor. Periodic work system; excellent mixing, transient

conditions, volume relationship with the degree of conversion and

reaction time. Flow system; equation of component continuity,

perfect mixing, steady state, design equation of the overflow tank

reactor, conventional reaction time.

2

Lec

14

Tubular reactor. Design equation for piston type system in steady

state. Comparison of volume and degree of conversion in continuous

reactors: tank and tubular.

2

Lec

15

Final test 2

Total hours 30

4

0


Proj 1 Volumetric gas properties determined from real gas state equations

third degree 2

Proj 2 Volumetric gas properties determined from the gas state equation

real Lee-Kesler 2

Proj 3 Work of compression and gas expansion 2

Proj 4 The functions of deviation from the perfect state: free energy, enthalpy,

enthalpy free, entropy, volatility 2

Proj 5 Getting to know with the Chemcad program 2

Proj 6 Process diagram. Simulation of stream diagrams 2

Proj 7 Analysis of the material balance of the system with the chemical reaction 2

Proj 8 Repetition of the material. Colloquium I 2

Proj 9 Analysis of the energy balance of the system with the chemical reaction 2

Proj

10

Influence of pressure and temperature on the course of the equilibrium

process 2

Proj

11

Analysis of the chemical process including kinetics 2

Proj

12

Simulation of the selected process 2

Proj

13

Simulation of the selected process - continuation 2

Proj

14

Simulation of the selected process - continuation 2

Proj

15

Project overview. Colloquium II 2

Total hours 30

TEACHING TOOLS USED


N2 Spreadsheet (Polymath program)

N3 Tables and graphs of substance properties

N4 Professional Chemcad program


Evaluation


semester),


semester end)

Educational effect


achievement

F1 (Project) PEK_U01 –

PEK_U02 partial colloquium I

F2 (Project) PEK_U02 – PEK_U05 partial colloquium II F3 (lectures) PEK_W01 –

PEK_W03 colloquium

4

1

C(projekt) = (F1 + F2)/2


PRIMARY LITERATURE:

[24] S. Kucharski, J. Głowiński, Podstawy obliczeń projektowych w technologii chemicznej, 3 wyd., Oficyna Wyd. PWr, Wrocław 2010

[25] Szarawara, J. Piotrowski, Podstawy teoretyczne technologii chemicznej, WNT, Warszawa 2010


[16] R.C. Reid, J.M. Prausnitz, B.E. Poling, The properties of gases and Liquids, 4th ed., Mcgraw-Hill, New

York 1987 [17] Praca zbiorowa, Przykłady i zadania do przedmiotu Podstawy technologii chemicznej, Oficyna Wyd.

PWr, Wrocław 1991 [18] W. Ufnalski, Wprowadzenie do termodynamiki chemicznej, Oficyna Wyd. PW, Warszawa 2004

SUBJECT SUPERVISOR


Prof.dr hab. inż. Józef Hoffmann, [email protected]

Dr inż. Ewelina Ortyl, [email protected]

Dr inż. Renata Kędzior, [email protected]


FOR SUBJECT

Fundamentals of chemical technology


lecture - all students of the Faculty of Chemistry

project-Chemistry, Chemical Technology, Engineering material

Subject

educational

effect





Subject



number***

(knowledge)

PEK_W01

K1Atc_W10, K1Aic_W10

K1Aim_W10,K1Ach_W11

K1Abt_W10

C1 Wy1 N1

PEK_W02


K1Aim_W10,K1Ach_W11

K1Abt_W10

C2 Wy2,Wy3 N1

PEK_W03


K1Aim_W10,K1Ach_W11

K1Abt_W10

C3 Wy4-Wy7 N1

PEK_W04


K1Aim_W10,K1Ach_W11

K1Abt_W10

C4 Wy4-Wy7 N1


4

2

(skills)

PEK_U01

K1Atc_U17, K1Aic_U09

K1Aim_U10, K1ach_U35

C3 Pr1,Pr2,Pr4 N2

PEK_U02



C2-C5 Pr1-Pr14 N2,N4

PEK_U03



C4 Pr5-Pr7 N3

PEK_U04



C5 Pr6 N4

PEK_U05



C5 Pr9-Pr14 N4



4

3

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Podstawy chemii fizycznej (kurs w jęz. ang.)

Name in English Fundamentals of physical chemistry Main field of study (if applicable) Chemia; Biotechnologia; Inżynieria chemiczna;

Inżynieria materiałowa; Technologia chemiczna.

Specialization (if applicable) -






Number of hours of





Form of crediting Examination Examination Examination

/ crediting

with grade*

Examination

/ crediting

with grade*

Examination

/ crediting


(X) final course X

Number of ECTS points 4 3





student contact (BK) classes 2 1.5



COMPETENCES

16. Elemental mathematics: Analysis I and II, algebra

17. Elemental physics: Physics I and II

18. Elemental chemistry: General chemistry, introductory inorganic chemistry

19. The English language

SUBJECT OBJECTIVES

Teaching fundamentals of:

C1 Application of thermodynamics for description of chemical reactions

C2 Elements of laboratory methods using the principles of phase equilibria:

distillation, crystallization, extraction, chromatography

C3 Electrochemical mesaurements in laboratory: potentiometry, conductometry,

4

4

polarography, amperometry

C4 Application of formal kinetic rate laws to describe rates of real world chemical

reactions



A person who passed the subject

PEK_W01 – knows fundamentals of thermodynamics

PEK_W02 – knows fundamentals of the description of phase transitions

PEK_W03– knows fundamentals of the functioning of electrochemical cells and the basic

behavior of ions in water solutions

PEK_W04– knows fundamentals of chemical kinetics

Relating to skills:


PEK_U01 – can solve elementary thermodynamics problems: computation of the reaction

heat, computation of the equilibrium constant

PEK_U02– can compute phase transition effects: vapor pressure depnding on the

conditions, the coposition of the distilate etc.

PEK_U02– can compute the electromotive force of cells, values of pH of solutions, solubility

of a salt in water etc.

PEK_U02– can calculate reaction rate constant, order of reaction and its activation energy

based upon results of the dependence of concentration on time at different

temperatures.

Relating to social competences:


PEK_K01 – possesses ability of combining information from disparate fields of science

(mathematics,physics, chemistry) to arrive at coherent conclusions

PEK_K02– is prepared to carry out computations involving elementary numerical methods

in physical chemistry and can assess objectively the validity of the obtained

result.

PROGRAMME CONTENT


Lec 1 Chemical thermodynamics. Heat and work. 1st law of

thermodynamics. Thermochemistry. 2

Lec 2 2nd

law of thermodynamics. Entropy, free energy and free enthalpy. 2

Lec 3 Chemical potential and chemical affinity. Chemical equilibrium.

van't Hoff's isobar. 2

Lec 4 Kinetic theory of gases. Equations of state. Real gases, fugacity. 2

Lec 5 Phase equilibria. Gibbs' phase rule. Phase equlibria in one-

component system (Clausius-Clapeyron equation). 2

Lec 6 Two-component systems. Liquid-vapor equilibrium (Raoult's and

Henry's equations). Distillation. Liquid-liquid equilibrium. Liquid-

solid equilibrium.

2

4

5

Lec 7 Three-component systems. Nernst's partition coefficient. Extraction. 2

Lec 8 Surface phenomena. Adsorption. Adsorption isotherms.

Chromatography. Surface tension. 2

Lec 9 Dispersed systems. Electrokinetic phenomena. Properties of

colloids. Transport phenomena: diffusion, viscous flow. 2

Lec

10

Electrochemistry. Electrochemical cells. Electromotive force.

electrochemical potentials. Cells as sources of energy. 2

Lec

11

Conductivity of electrolyte solutions. Electrolysis. Polarography.

Electrochemical methods in chemical analysis. 2

Lec

12

Chemical kinetics. Reaction rate. Formal kinetics: reaction order.

Non-elementary reactions. 2

Lec

13

Temperature dependence of reaction rates. Activation energy.

Theoretical description. 2

Lec

14

Homogeneous and heterogeneous catalysis. Autocatalytic reactions.

Kinetics of ionic reactions. Kinetics of reactions in multiphase

systems.

2

Lec

15

Kinetics of reactions in solids / Osmotic phenomena. 2

Total hours 30


Cl 1 1st law of thermodynamics. Calculations of work, heat, and changes of

internal energy and enthalpy. 2

Cl 2 Calculating heats of chemical reactions. Hess and Kirchhoff's laws. 2 Cl 3 Entropy, free energy and free enthalpy. 2

nd law of thermodynamisc applied

to chemical reactions. Chemical affinity of reaction. Chemical potential of

a component.

2

Cl 4 Chemical equilibria. Equilibrium constants, temperature ans pressure

dependences. van't Hoff's isobar. Equilibria in real systems. 2

Cl 5 Phase equilibria in one-component systems. Phase diagrams. Clausius-

Clapeyron equation. 2

Cl 6 Phase equilibria in multicomponent systems. Phase rule. 2

Cl 7 Two component systems: two liquids and liquid-vapour equilibria. Raoult

and Henry’s laws. Distillation. Two-component solid-liquid systems.

osmotic phenomena. Three-component systems. Gibbs's triangle.

2

Cl 8 1st written test 2

Cl 9 Surface phenomena. Adsorption on solid surfaces. Surface tension.

Szyszkowski and Gibbs equations. 2

Cl 10 Ionic equilibria in solutions. Activities. Calculations of pH and of

concentrations in acid-base equilibria. 2

Cl 11 Electromotive force and electrode processes. Reactions and Nernst

equations for typical half-cells. Calculating thermodynamic functions from

EMF. Calculating solubility product from EMF.

2

Cl 12 Electrical conduction of electrolyte solutions. Determination of ion

mobilities. Calculations of electrolytic conductivity and molar conductivity

of strong and weak electrolytes.

2

Cl 13 Determination of solubility product from measurements of conductivity.

Determination of transfer numbers. 2

Cl 14 Formal kinetics of elementary reactions. Determination of orders and rate 2

4

6

constants of simple reactions.

Cl 15 Final (2nd) test 2

Total hours 30

TEACHING TOOLS USED

N1 Lecture: multimedial presentation

N2 Lecture: multiple choice test

N3 Classes: a set of computational problems, presented to teh students for individual

elaboration and discussed during the class

N4 Class: a traditional written test


Evaluation


semester),


semester end)

Educational effect


achievement

F1 PEK_U01,

PEK_U02

Test 1

F2 PEK_U03,

PEK_U04

Test 2

F3 PEK_W01

PEK_W02

PEK_W03

PEK_W04

PEK_K01

PEK_K02

Exam

P= (3/5)(F1+F2)+(4/10)F3


PRIMARY LITERATURE:

[26] Peter Atkins, Julio De Paula, "Atkins' Physical Chemistry", Eighth edition, Oxford

University Press, Oxford 2006

[27] Peter Atkins and Julio de Paula, „Atkins' Physical Chemistry”, Ninth Edition, Oxford

University Press, Oxford 2009

[28] Charles Trapp, Marshall Cady, and Carmen Giunta, „Student's solutions manual to

accompany Atkins' Physical Chemistry 9/e”, Oxford University Press, Oxford 2010


[19] H. Kuhn i H.-D. Försterling, Principles of Physical Chemistry. Understanding

Molecules, Molecular Assemblies, Supramolecular Machines, J. Wiley, Chichester

1999

[20] Clifford E. Dykstra, Physical Chemistry: A Modern Introduction, CRC Press, 2012

4

7

SUBJECT SUPERVISOR


Prof. Marek Samoć, [email protected]


FOR SUBJECT

Fundamentals of physical chemistry


Biotechnology

Subject

educational

effect





Subject



number***

(knowledge)

PEK_W01

K1Abt_W08, K1Aic_W08

K1Aim _W08, K1Atc_W08 C1 Wy1-Wy4 N1, N2

PEK_W02 K1Abt_W08, K1Aic_W08






(skills)

PEK_U01

K1Abt_U15, K1Aic_U08

K1Aim_U08, K1Atc_U08 C1 Cw1-Cw5 N3, N4

PEK_U02 K1Abt_U15, K1Aic_U08






(competences)

PEK_K01 C1-C5 Cw1-Cw15 N1, N2, N3, N4

PEK_K02 C1-C4 Cw1-Cw15 N1, N2, N3, N4



4

8

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Inżynieria genetyczna

Name in English Genetic Engineering Main field of study (if applicable) Biotechnology







Number of hours of


University (ZZU) 60




with grade*


(X) final course









COMPETENCES

20. Basics of molecular biology and biochemistry.

21. Basics of laboratory work.

SUBJECT OBJECTIVES

C1 Familiarizing students with basic techniques used for DNA recombination

C2 Acquiring the theoretical and practical skills necessary to molecular cloning

C3 Familiarizing students with basic expression systems

C4 Acquiring the theoretical and practical skills necessary to overexpression of protein in

bacteria

C5 Familiarizing students with recombinant DNA technologies used in biotechnology

medicine, agriculture archaeology

C6 Familiarizing students with techniques used for gene/genome structure analysis

C7 Familiarizing students with methods needed for analysis of expression and function of

genes and genomes

4

9


Relating to knowledge: PEK_W01 – Student describes and explains basic molecular tools needed for construction and

analysis of recombinant DNA molecules

PEK_W02 – Student describes and explains structural and functional elements of vectors

PEK_W03 – Student describes and explains techniques needed for isolation, amplification and

biochemical/biophysical characterization of DNA

PEK_W04 – Student describes and explains DNA transfer techniques

PEK_W05 – Student describes and explains genes/genome sequencing techniques

PEK_W06 – Student describes and explains methods needed for the analysis of gene/genome

expression

PEK_W07 – Student describes and explains various practical applications of genetic engineering in

biotechnology, medicine, agriculture and archaeology.

Relating to skills:

PEK_U01 – Student is able to plan and conduct restriction digestion experiment

PEK_U02 – Student is able to conduct agarose gel electrophoresis and to interpret the results

PEK_U03 – Student is able to plan PCR experiment (starter design, PCR reaction setup)

PEK_U04 – Student is able to use DNA isolation kits (Gel-out, Clean-up)

PEK_U05 – Student is able to prepare competent bacterial cells

PEK_U06 – Student is able to setup and conduct DNA ligation reaction

PEK_U07 – Student is able to setup and conduct DNA transfer into bacteria

PEK_U08 – Student is able to setup and analyse (SDS-PAGE) overexpression of recombinant

protein in bacteria.


Lab 1 Familiarizing students with genetic engineering laboratory course. 6

Lab 2 Digestion of pGEX-2T plasmid vector with BamHI restrcition

endonuclease

6

Lab 3 Agarose gel electrophoresis of linearized and dephosphorylated pGEX-2T

plasmid vector

6

Lab 4 PCR of EcRDBD 6

Lab 5 Isolation of PCR product – Clean-up protocol 6

Lab 6 Preparation of competent XL1-Blue cells 6

Lab 7 Ligation of pGEX-2T/BamHI plasmid vector with EcRDBD fragment

digested with BamHI

6

Lab 8 Overexpression of EcRDBD (cloned in pGEX2T) in XL1-Blue cells 6

Lab 9 Analysis of EcRDBD expression using SDS-PAGE 6

Lab 10 Test 6

Total hours 60

TEACHING TOOLS USED

N1 Performing experiment

N2 Short theoretical introduction to experiment


N4 Solving questions and problems

N5 Preparing reports on the experiments

5

0


Evaluation


semester),


semester end)

Educational effect number Way of evaluating educational effect

achievement

C (lecture) PEK_W01 – PEK_W08 Multiple-choice test

C (lecture) = 3,0 if = 60,0 – 70,0 points

3,5 if = 70,1 – 75,0 points

4,0 if = 75,1 – 80,0 points

4,5 if = 80,1 – 85,0 points

5,0 if = 85,1 – 90,0 points

5,5 if = 90,1 – 100,0 points

F1 (laboratory) PEK_U01- PEK_U08 Final test

F2 (laboratory) PEK_U01- PEK_U08 Reports on the experiments

C (laboratory) = 3,0 if (F1+F2) = 60,0 – 70,0 points

3,5 if (F1+F2) = 70,1 – 75,0 points

4,0 if (F1+F2) = 75,1 – 80,0 points

4,5 if (F1+F2) = 80,1 – 85,0 points

5,0 if (F1+F2) = 85,1 – 90,0 points

5,5 if (F1+F2) = 90,1 – 100,0 points


PRIMARY LITERATURE:

[29] Brown, T.A. "Gene Cloning and DNA Analysis: An Introduction. John Wiley & Sons, 6th

edition

[30] Experiment manuals available on the course-specific website only to qualified students



edition

[22] Brown, T.A. "Genomy" PWN 2009

[23] Węgleński, P. "Genetyka molekularna" PWN (wydanie nowe)

[24] Berg, J.M., Tymoczko, J.L., Stryer, L. „Biochemia” PWN SA 2005/6 (tłumaczenie 6 wydania

amerykańskiego)

[25] Berg, J.M., Tymoczko, J.L., Stryer, L. „Biochemistry” W.H. Freeman and Co., New York –

7th edition

[26] http://www.blackwellpublishing.com/genecloning/

SUBJECT SUPERVISOR


Prof. dr hab. inż. Andrzej Ożyhar, [email protected]

5

1


FOR SUBJECT

………Genetic engineering………….


………Biotechnology…………….

Subject

educational

effect





Subject



number***

(knowledge)

PEK_W01 K1Abt_W25 C1

Lec1, Lec2,

Lec3, N3

PEK_W02 K1Abt_W25 C1, C2, C3, C4 Lec2, Lec4,

Lec5, Lec2 N3

PEK_W03 K1Abt_W25 C1, C2 Lec3, Lec6,

Lec8 N3

PEK_W04 K1Abt_W25 C2, C3, C4 Lec4, Lec5,

Lec10 N3

PEK_W05 K1Abt_W25 C1, C6 Lec7, Lec9,

Lec11 N3

PEK_W06 K1Abt_W25 C1, C7 Lec10, Lec12 N3

PEK_W07 K1Abt_W25 C5 Lec14, Lec14,

Lec15 N3

(skills)

PEK_U01 K1Abt_U26 C1, C2 La1, La2

N1, N2, N3,

N4, N5

PEK_U02 K1Abt_U26 C1, C2 La2, La3, La4 N1, N2, N3, N5

PEK_U03 K1Abt_U26 C1, C2, C4 La4 N1, N2, N3,

N4, N5

PEK_U04 K1Abt_U26 C1, C2 La3, La5 N1, N2, N5

PEK_U05 K1Abt_U26 C2, C3, C4 La6 N1, N2, N3, N5

PEK_U06 K1Abt_U26 C1, C2 La7 N1, N2, N3,

N4, N5

PEK_U07 K1Abt_U26 C1, C2, C3, C4 La7 N1, N2, N5

PEK_U08 K1Abt_U26 C4 La8, La9 N1, N2, N3, N5


*** - from tables above

5

2

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Procesy Cieplne

Name in English Heat Transfer Processes Main field of study (if applicable) Chemical Engineering and Processing







Number of hours of





Form of crediting Examination

/ crediting

with grade*

Examination

/ crediting

with grade*

Examination

/ crediting

with grade*

Examination

/ crediting

with grade*

Examination

/ crediting


(X) final course





student contact (BK) classes 1 1 1



COMPETENCES

22. Basic knowledge of mathematics

23. Knowledge of chemistry at the high school level

24. Knowledge of physics at the high school level

SUBJECT OBJECTIVES

C1 Acquirement of the basic knowledge about the steady and transient heat transfer by

conduction, convection and radiation

C2 Acquirement of the basic knowledge about the design and selection of heat

exchangers

C3 Learning how to perform basic calculations of heat transfer and heat exchangers

C4 Obtaining basic skills of measurement of heat transfer

5

3



The person who has passed this subject:

PEK_W01 - has a basic knowledge of heat transfer by conduction,

PEK_W02 - has a basic knowledge about heat transfer by convection,

PEK_W02 - has a basic knowledge about heat transfer by radiation,

PEK_W04 - has a basic knowledge about heat transfer coefficients,

PEK_W05 - knows the basics of modeling of unsteady state heat transfer,

PEK_W06 - has a knowledge of methods of heat exchangers designing.

Relating to skills:

The person who has passed this subject:

PEK_U01 - can perform calculations related to heat transfer by conduction, convection and

radiation,

PEK_U02 - can perform calculations related to the heat transfer coefficients,

PEK_U03 - can design basic types of heat exchangers,

PEK_U04 - can design and conduct experiments necessary to calculate the heat transfer.

PROGRAMME CONTENT


Lec 1 Types of heat transfer 2

Lec 2 Heat transfer between two fluids separated by a solid wall 2

Lec 3 Thermal isulation 2

Lec 4 Unsteady state heat conduction - introduction 2

Lec 5 Unsteady state heat conduction – basics 2

Lec 6 Heat transfer by convection - introduction 2

Lec 7 Heat transfer by convection - analysis 2

Lec 8 Analogy between momentum and heat transfer 2

Lec 9 Heat transfer by radiation 2

Lec 10 Heat exchangers - basics 2

Lec 11 Designing of heat exchangers 2

Lec 12 Unsteady heat transfer in liquids 2

Lec 13 Concentration of solutions of non-volatile substances 2

Lec 14 Selection of a heat exchanger 2

Lec 15 Computational Fluid Dynamics in the design process of heat devices 2

Total hours 30


Lab 1 Introduction 3

Lab 2 Heat transfer in the air cooler 3

Lab 3 Heat transfer in the shell-and-tube heat exchanger 3

Lab 4 Unsteady heat transfer in solid 1 3

5

4

Lab 5 Heat transfer in the plate heat exchanger 3

Lab 6 Heating and cooling of liquids in conditions of natural convection 3

Lab 7 Heat transfer in the thin layer evaporator with gravitational liquid

flow 3

Lab 8 Heat transfer in the double-pipe heat exchanger 3

Lab 9 Heat transfer during boiling 3

Lab 10 Unsteady heat transfer in solid 2 3

Total hours 30


Proj 1 Heat conduction in flat and annular walls 4

Proj 2 Thermal insulation 2

Proj 3 Heat transfer in conditions of natural convection 2

Proj 4 Heat transfer in conditions of forced convection 2

Proj 5 Heat transfer in conditions of boiling and condensation 2

Proj 6 Test 2

Proj 7 Heat transfer between two fluids separated by flat and annular

walls 4

Proj 8 Heat transfer by radiation 2

Proj 9 Designing of the thermal insulation of pipelines 2

Proj10 Project of a heat exchanger 6

Proj 11 Test 2

Total hours 30

TEACHING TOOLS USED


N2 Tasks solving

N3 Project making

N4 Carrying out experiments

N5 Report making


Evaluation


semester),


semester end)

Educational effect


achievement

C (Lecture) PEK_W01 –

PEK_W06

Final Exam

F2 (laboratory) PEK_U02,PEK_U04 Test, report

F3 (laboratory) PEK_U02, PEK_U04 Test, report



5

5






C (laboratory) = (F2+F3+F4+F5+F6+F7+F8+F9+F10)/9

F1 (project) PEK_U01, PEK_U02 Test 1

F2 (project) PEK_U02, PEK_U03 Test 2

C(project) = (F1+F2)/2


PRIMARY LITERATURE:

[31] A. Kmieć, Procesy cieplne i aparaty, Oficyna Wydawnicza Politechniki Wrocławskiej,

Wrocław, 2005.

[32] A. Skoczylas, Przenoszenie ciepła, Oficyna Wydawnicza Politechniki Wrocławskiej,

Wrocław, 1999.

[33] A. Kawala, M. Pająk, J. Szust, Zbiór zadań z podstawowych procesów inżynierii

chemicznej. Część 2. Przenoszenie ciepła, Wydawnictwo Politechniki Wrocławskiej,

Wrocław, 1987.

[34] http://www.iic.pwr.wroc.pl/index.php/dydaktyka/43-kierunkowe/procesy-cieplne


[27] T. Hobler, Ruch ciepła i wymienniki, Wydawnictwo Naukowo Techniczne,

Warszawa, 1979.

[28] R.H. Perry, Perry’s Chemical Engineers’ Handbook, McGraw-Hill, 1997.

SUBJECT SUPERVISOR


Wojciech Ludwig, [email protected]


FOR SUBJECT

Heat Transfer Processes


Chemical Engineering and Processing

Subject

educational

effect





Subject

objectives***

Programme

content***

Teaching tool

number***

(knowledge) K1Aic_W22 C1 Lec1, Lec5 N1

5

6

PEK_W01

PEK_W02 K1Aic_W22 C1 Lec1, Lec6,

Lec7, Lec12 N1

PEK_W03 K1Aic_W22 C1 Lec9, Lec15 N1


Lec7 N1


Lec15 N1


Lec14, Lec15 N1

(skills)

PEK_U01 K1Aic_U25 C3

Lab2-Lab10

Pr1, Pr2, Pr8 N2, N3


Lab2, Lab3,

Lab5-Lab9

Proj3-Proj5,

Proj7

N2, N3

PEK_U03 K1Aic_U25 C3 Proj10, Lab3,

Lab8 N2, N3

PEK_U04 K1Aic_U26 C4 Lab2-Lab10 N4, N5



5

7

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Mikrobiologia przemysłowa

Name in English Industrial microbiology Main field of study (if applicable) Biotechnology




Subject code BLC014003



Number of hours of


University (ZZU)

45




with grade


(X) final course





student contact (BK) classes

1.5



COMPETENCES

25. Biological background at academic level.

26. Microbiological background at academic level

27. Laboratory practice in microbiological work.

SUBJECT OBJECTIVES

C1 The understanding morphology and physiology of microbes of industrial

importance.

C2 The learning of methods of microbes isolation from natural sources, their

improvements and identification procedures.

C3 The acquisition of knowledge about methods of bioprocess and raw materials used

in biotechnology.

C4 The learning of microbes settled raw materials used in food industry and foodstuffs.

C5 The learning of possible methods used in evaluation of microbial contamination in

samples of various origin.

C6 The learning of practical techniques for the evaluation of basic microbial properties

5

8



Student:

PEK_W01 – has the knowledge about physiology and morphology of industrially used

microbes

PEK_W02 – know the techniques of microbes isolation, identification and modification

PEK_W03 – know the methods of bioprocess course and types of raw materials used in

biotechnology

PEK_W04 – has a knowledge about the microorganisms settled food materials

PEK_W05 – know how to demonstrate the presence of microorganisms in various type

materials.

PEK_W06 – can characterize microbes caused some infection of digestive system

Relating to skills:

Student:

PEK_U01 – know how to plane and carry out the experiment procedure led to examine of

particular enzymatic activity in microbial cells and can effectively analyze

obtained results

PEK_U02 – can disrupt biological material of different origin using various techniques and

know how to check results of this process.

PEK_U03 – can isolate new microbial strain from natural sources and carry out the basic

characteristic of it.

PEK_U04 – know the procedures of the evaluation of microbial sensitivity level on

different types of antibiotics

PEK_U05 – can analyze microbial contamination of sample

PEK_U06 – can immobilize microbes and know how to use this kind of biocatalysts in

desired process


Lab 1 Pass/fail evaluation options. Secured work with microbes of different

origin in laboratory. Description of basic tools of work. 3

Lab 2 Disruption of microorganisms. Mechanical techniques – disintegration

of baker yeast cells using Beat-beater machine and grinding of yeast

cells with sand using mortar and pestle. 3

Lab 3 Disruption of microorganisms. Non-mechanical techniques - baker

yeast disintegration by freezing/defreezing method and chemical

disruption process. 3

Lab 4 Immobilization of microorganisms. Encapsulation of yeast cells in

alginate. 3

Lab 5 Biocatalysis. The comparison of reductive activity of free and

immobilized biocatalyst toward acetophenone. Ethanol production by

free yeast cells or immobilized biocatalysts. 3

Lab 6 Antibiotics produced by prokaryotic and eukaryotic

microorganisms. Antibiotic-producing fungi – screening procedures.

Antibiotic-producing Actinomycetales – screening procedures.

Sensitivity test.

3

5

9

Lab 7 Elaboration of experiments results. Antibiotics. Sensitivity of chosen

bacterial strains on commercially used antibiotics. The evaluation of

minimum inhibitory concentration of antibiotics on microorganisms.

Gradient -plate method of evaluation of antibiotic effect of microbial

growth. Synergic action of chemotherapeutics.

3

Lab 8 Elaboration of experiments results. Isolation of new strains of

microorganisms. Isolation of lipolytic microbes from natural sources,

using enrichment techniques. Assays for lipases activity. 3

Lab 9 Elaboration of experiments results. Enzymes. The ability of

microorganisms to produce exo-amylases. Proteolytic activity of

microorganisms. Lipolytic activity of bacterial strains. 3

Lab 10 Elaboration of experiments results. Enzymes. Assay of dehydrogenases

activity in plant material. 3

Lab 11 Food analysis. Assays of fungal and bacterial contamination of food.

Evaluation of contaminant presence in food. 3

Lab 12 Elaboration of experiments results. Evaluation of water quality. Assays

of fungal and bacterial contamination of water samples. Coli index.

Cellulases-producing microbes in water – isolation methods. 3

Lab 13 Elaboration of experiments results. Additional laboratory allowing

catching up. 3

Lab 14 Crediting with grade – 1 st term. (Colloquium and practical part) 3

Lab 15 Crediting with grade – 2 nd term. (Colloquium and practical part) 3

Total hours 45

TEACHING TOOLS USED

N1 Classical lecture with multimedial presentation.

N2 Practical work.


Evaluation


semester),


semester end)

Educational effect


achievement

C PEK_W01-

PEK_W06

Crediting of grade – electronic colloquium

C PEK_U01-

PEK_U06

Crediting of grade (Colloquium and

practical part)

6

0


PRIMARY LITERATURE:

[29] Mikrobiologia techniczna. Red. Z. Libudzisz, K. Kowal, Z. Żakowska, PWN,

Warszawa, 2008


[1] Biotechnologia Żywności. red. W. Bednarski, A. Reps, WNT, Warszawa, 2003

[2] Podstawy Biotechnologii Przemysłowej. red. W. Bednarski, J. Fiedurek, WNT,

Warszawa, 2007

SUBJECT SUPERVISOR


Magdalena Klimek-Ochab PhD, [email protected]


FOR SUBJECT

Industrial microbiology


Biotechnology

Subject

educational

effect





Subject

objectives***

Programme

content***

Teaching tool

number***

knowledge

PEK_W01 K1Abt_W20 C1 Lec 1-3, Lec 13 N1

PEK_W02 K1Abt_W20 C2 Lec 4-6 N1

PEK_W03 K1Abt_W20 C3 Lec 7, Lec 8 N1

PEK_W04 K1Abt_W20 C4 Lec 9 N1

PEK_W05 K1Abt_W20 C5 Lec 11- Lec 12 N1

PEK_W06 K1Abt_W20 C4 Lec 10 N1

skills

PEK_U01

K1Abt_U21 C6 Lab9, Lab10 N2

PEK_U02 K1Abt_U21 C3 Lab2, Lab3 N2

PEK_U03 K1Abt_U21 C2 Lab1, Lab8,

Lab14, Lab15

N2


PEK_U05 K1Abt_U21 C5 Lab11-Lab12 N2




6

1

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish: Technologie informacyjne

Name in English: Information technologies Main field of study (if applicable): Erasmus students


Level and form of studies: 1nd

level, full-time


Subject code TIC024001



Number of hours of


University (ZZU) 30




with grade


(X) final course




points for direct teacher-student

contact (BK) classes 1



1. Ability to basic computer skill

2. Ability to use word processing and spreadsheet

SUBJECT OBJECTIVES

C1 Obtaining knowledge of the foundations of computer science.

C2 Developing skills in information technologies.

C3 Obtaining writing skills of simple algoritms.

C4 Understanding the elements of a selected programming language.

6

2



PEK_U01 – Ability to search for information on the Internet and formulate queries in a

database.

PEK_U02 – Ability to use text editors and chemical equations to the extent necessary in

engineering work

PEK_U03 – Ability to use spreadsheets to the extent necessary in engineering work

PEK_U04 – Ability to formulate simple algorithm

PEK_U05 – Ability to write a simple calculation program

PROGRAMME CONTENT


La1 Overview of the course, student mail, Moodle. Database, information

retrieval on the web. 2

La2 The aptitude test in using Microsoft Word. 2

La3 Equation Editor of Microsoft Word. 2

La4 ISIS Draw. 2

La5 Test I. The aptitude test in using Microsoft Excel. 2

La6 Microsoft Excel: address types of cells, formulas and functions, graph

of experimental data and the polynomial fitting. 2

La7 Microsoft Excel Solver: solving nonlinear equations and optimization

problems. 2

La8 Algorithms. Flowchart. Creating simple algorithms and writing them

using flowcharts. 2

La9 Test II. Number systems and conversion of numbers between the

systems. 2

La10 Introduction to Matlab. Interactive working. Arithmetic operations.

Variables. 2

La11 Writing simple computer programs on the basis of previously

developed algorithms. 2

La12 Decision-making in a program 2

La13 Cyclic calculations. 2

La14 Applications of cyclic calculations. 2

La15 Repetition of material. Test III. 2

Total hours 30

TEACHING TOOLS USED

N1 The introduction with multimedia presentation.

N2 Unassisted solving the problems posed during the course with using appropriate

computer programs.

6

3


Evaluation


semester),


semester end)


achievement

F1(laboratory) PEK_U01 – PEK_U02,

PEK_U4

mean value from 3small written exams

F2 (laboratory) PEK_U03 The task for an evaluation.


PRIMARY LITERATURE:

[1]. Manuals from Microsoft.

[2]. Any manual fundamentals of computer science.

[3] Selected manual on programming language (given by the teacher).

SUBJECT SUPERVISOR


Dr hab. inż. Jan Kapała [email protected]


FOR SUBJECT

Information technologies B


Chemistry

Subject

educational effect Correlation between subject




Subject



number***

(skills)

PEK_U01

K1Abt_U08, K1Ach_U38,

K1Aic_U25, K1Aim_U12, C1, C2 Lab1-La3 N1, N2

PEK_U02 K1Atc_U37 C1, C2 Lab4 N1, N2

PEK_U03 K1Abt_U08, K1Ach_U38,

K1Aic_U25, K1Aim_U12, C3 Lab5 N1, N2

PEK_U04 K1Atc_U37 C4 Lab6, Lab7 N1, N2 ** - enter symbols for main-field-of-study/specialization educational effects


6

4

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Materiałoznawstwo

Name in English Materials science Main field of study (if applicable) Chemical technology

Chemical and processing engineering




Subject code IMC024008



Number of hours of


University (ZZU) 30




/ crediting

with grade*


(X) final course








COMPETENCES

28. Chemistry and physics - basic

SUBJECT OBJECTIVES

C1 Introducing the students to the repartition of engineering materials

C2 Learning the selection rules for a material to a definite application

C3 Acquisition of information about usable properties of engineering materials

C4 Understanding the relationship material/structure/production method

6

5



Any person who has got a credit of the subject:

PEK_W01 – knows basic sorts of engineering materials, bad and good sides of these;

PEK_W02 – understands the selection rules for a material to a definite application;

PEK_W03 – knows the definitions, importance and means of determination of the main

mechanical properties of the materials as the deciding factors for applications

in practice;

PEK_W04 – has acquired basic information about correlations between materials'

properties, structure and production method;

PEK_W05 – has acquired basic knowledge about metallic material structure, phase

equilibria and transformations;

PEK_W06 – knows the basics of rheology in the linear viscoelasticity of polymer materials;

PEK_W07 – knows the basics of polymer processing methods.

PROGRAMME CONTENT


Lec 1 Types of engineering materials: basic advantages and disadvantages

of metals, ceramics and plastics. Composites. 2

Lec 2 Types of crystalline materials through the ages. Recent

achievements and trends in production of new materials:

nanomaterials, shape memory materials etc.

2

Lec 3 Atom structure in light of present-day studies. Types and energies of

chemical bonding. Importance of binding energy in properties of

materials. Chemical bonds dominating throughout the respective

types of engineering materials.

2

Lec 4 Basic information about the crystal structure of materials. Crystal

structure of metals. Unit cell. Correlations between the production

process, crystal structure and properties of materials. Crystalline and

amorphous materials.

2

Lec 5 Mechanical properties of engineering materials. Stress and strain.

Elastic and plastic deformations. Static tensile test. Hardness. Impact

strength. Cracking resistance. Fatigue. Creep.

2

Lec 6 Crystal structure defects. Substitution and interstitial solid solutions.

The crystallographic structure of iron and steel. Metals and alloys.

Homogenous and heterogenous alloys.

2

Lec 7 Gibbs phase rule. Phase diagrams for binary systems with a perfect-,

partial-, and completely lacking intersolubility. 2

Lec 8 Alloy- and non-alloy steels: obtaining, properties, and applications.

Systems of marking the steels. Constructional and tool steels. Cast

irons. The system iron-carbon. Non-ferrous metal alloys.

2

Lec 9 Basic information about corrosion of metals. Methods of corrosion

protection. 1

Lec 10 Partial test 1

Lec 11 Synthetic engineering materials; historical outline, milestones in

discoveries. 2

6

6

Lec 12 Conception of the macroparticle (synthesis methods, radical

polymerization, degree of polymerization, polycondensation). 2

Lec 13 Amorphous and semicrystalline polymers, crosslinked polymers

(structural models, glass transition temperature, melting point). 2

Lec 14 Rheological models (the Maxwell model, Kelvin-Voigt model,

Maxwell three-parameter model; creep, tension relaxation, plastic

deformation recovery).

2

Lec 15 Typical machinery to process polymer materials. The operating

principle of: injection molding machine; extruder; two-high rolling

mill; calender roller; hydraulic press. Rotomolding.

2

Lec 16 PCW example of polymer modification (relationship between

structure, composition, and functional properties). 1

Lec 17 Partial test 1

Total hours 30

TEACHING TOOLS USED

N1 Informative lecture including a multimedia presentation


Evaluation


semester),


semester end)

Educational effect


achievement

F1 (lecture) PEK_W01 –

PEK_W05

Part test-colloquium

F2 (lecture) PEK_W02,

PEK_W04,

PEK_W06,

PEK_W07

Part test-colloquium

C (lecture) - condition to be credited: positive grades from both partial tests.

3,0 if (F1 +F2) = 6,0 – 6,5

3,5 if (F1 +F2) = 7,0 – 7,5

4,0 if (F1 +F2) = 8,0

4,5 if (F1 +F2) = 8,5 – 9,0

5,0 if (F1 +F2) = 9,5 – 10,0

5,5 if (F1 +F2) = 10,5 – 11,0

6

7


PRIMARY LITERATURE:

[35] M. Blicharski, Wstęp do inżynierii materiałowej, WNT, Warszawa, 2003.

[36] W.D. Callister Jr, Materials Science and Engineering, Jihn Willey & Sons Inc., New

York, 1991.

[37] D. Żuchowska, Polimery konstrukcyjne, WNT, Warszawa, 1995.

[38] W. Szlezyngier, Tworzywa sztuczne, Oficyna Wydawnicza Politechniki

Rzeszowskiej, Rzeszów, 1996.


[30] L.A. Dobrzański, Podstawy nauki o materiałach i metaloznawstwo, WNT, Gliwice,

Warszawa, 2002.

[31] M. Blicharski, Inżynieria materiałowa. Stal, WNT, Warszawa, 2004.

[32] W. Królikiewicz, Polimerowe materiały specjalne, Wydawnictwo Politechniki

Szczecińskiej, Szczecin, 1998.

SUBJECT SUPERVISOR


Prof. dr hab. inż. Bogdan Szczygieł; [email protected]

Prof. dr hab. inż. Jacek Pigłowski; [email protected]


FOR SUBJECT

Materials science


Chemical technology

Chemical and processing engineering

Subject

educational

effect





Subject



number***

(wiedza)

PEK_W01 K1Atc_W19, K1Aic_W15 C1

Lec1, Lec 2,

Lec 11 N1

PEK_W02 K1Atc_W19, K1Aic_W15 C2 Lec 3, Lec 8,

Lec 9, Lec 16 N1, N2

PEK_W03 K1Atc_W19, K1Aic_W15 C3 Lec 5, Lec 13 N1

PEK_W04 K1Atc_W19, K1Aic_W15 C4 Lec 4, Lec 12 N1

PEK_W05 K1Atc_W19, K1Aic_W15 C4 Lec 6, Lec 7 N1, N2

PEK_W06 K1Atc_W19, K1Aic_W15 Lec 14 N1

PEK_W07 K1Atc_W19, K1Aic_W15 Lec 15 N1





6

8

FACULTY OF CHEMICAL ENGINEERING

SUBJECT CARD

Name in Polish Pomiary w aparaturze procesowej

Name in English Measurements in chemical equipment Main field of study (if applicable): Chemical Engineering

Specialization (if applicable):

Level and form of studies: 1st level, full time


Subject code: ICR024024

Group of courses NO


Number of hours of organized classes in


Number of hours of total student workload

(CNPS) 30 60

Form of crediting test crediting with

grade

For group of courses mark (X) final course Number of ECTS points 2 2

including number of ECTS points for practical (P)

classes 2

including number of ECTS points for direct teacher-

student contact (BK) classes 1,5 2



Competences in the field of mathematics and physics confirmed by positive assessments on the

certificate of upper secondary school graduation.

SUBJECT OBJECTIVES

C1. Basic knowledge about metrology terms, error theory and measurement uncertainty theory,

instruments to measure mean and RMS value currents and voltages..

C2. Make students aware of the possibility of using measuring circuits realizing different

measurement methods for measuring basic electrical and non-electrical quantities.



PEK_W01 Students knows basic terms of metrology. Student has knowledge in the field of

measurement errors: systematical, random and mistakes with measuring errors interpretation on

the base of instrument class knowledge..

PEK_W02 Student has knowledge about using and calculating uncertainty type A, B, total and

extended.

PEK_W03 Students knows the construction, operation principle and processing characteristics of

the most common measuring transducers. He knows the rules of physical quantities

processing into electrical quantities.

PEK_W04 Students have basic knowledge of the dynamic characteristics of sensors and

transducers. He knows the mathematical models of sensors and transducers.

6

9

relating to skills:

PEK_U01 Student is able to make current and voltage measurements with analog and digital

instruments and can calculate measurement result using the uncertainty theory.

PEK_U02 Student has the ability in oscilloscope measurements for sinusoidal and distorted

signals for high frequencies.

PEK_U03 Student is able to correctly select an instrument to measuring non-electrical quantities.

PEK_U04 Student is able to use the tool to temperature, pressure, stress, vibration, moisture

content, chemical composition, flow rates of gases and liquids measure.

PEK_U05 Student has the skills to assess the impact of external factors on the result. He can

estimate the measurement method error and make a correction.

relating to social competences:

PEK_K01 Student is aware of their own responsibility for their work and a willingness to comply with

the principles of teamwork.

PEK_K02 Student searches information and can subject them to critical analysis.

PROGRAMME CONTENT

Form of classes - lecture Number of

hours

Lec 1 Basic terms of metrology. Measurement errors of analogue and digital

instruments. Instruments errors and classes. Systematical and random errors,

mistakes.

2

Lec 2 Measurement uncertainty. Uncertainty type A, type B. Total uncertainty.

Statistical distributions: Normal and Student.

2

Lec 3 Uncertainty of direct measurements. Uncertainty of indirect measurements.

Calculation examples.

2

Lec 4 Processing of non-electrical quantities into electrical signals - general issues.

Analogue to digital transducers of non-electrical quantities. Measurements of

linear and angular displacement, measurements of vibration.

2

Lec 5 Strain gauge transducers, torque measurement, force measurements.

Measurement of gas and liquid flow rates. Pressure measurements

2

Lec 6 Phametric and conductometric measurements, Measurements of chemical

composition. Humidity measurements.

2

Lec 7 . Temperature measurement, temperature measurement methods, resistance

and thermoelectric thermometers. Measuring methods for the temperature of

solids, gases and liquids. Temperature measurements in industrial equipment.

2

Lec 8 Summary and credit of the subject 2

Total hours 15

Form of classes - class Number of

hours

Cl 1

Cl 2


hours

La1 Presentation of safety regulations and laboratory rules. Establish complete

the course rules. Write of the measurement result learning.

2

La2 Analog instruments uses to measure voltages and currents. Determination

of relative and absolute errors. Determination of the measurement result

2

7

0

uncertainty.

La3 Digital instruments uses to measure voltages and currents. Determination

of relative and absolute errors. Determination of the measurement result

uncertainty.

2

La4 Measurements of sine and distorted waves by using an oscilloscope. 2

La5 Understanding the basic concepts of statistics and probability theory used

in the assessment of the measurement accuracy with random errors.

2

La6 Power measurements. 2

La7 Frequency and phase shift measurements. 2

La8 Temperature measurements - determining characteristics of temperature

sensors.

2

La9 Strain gauge measurements – sensor properties, force sensors tests. 2

La10 Pressure measurements. 2

La11 Liquid pH and conductivity measurements. 2

La12 Gas flow measurements 2

La13 Humidity measurements 2

La14 Determination of proximity (distance) sensor characteristics and linear and

angular displacement sensors.

2

La15 Grading 2

Total hours 30

Form of classes - project Number of

hours

Proj 1

Total hours

Form of classes - seminar Number of

hours

Sem 1

Total hours

TEACHING TOOLS USED

N1. Lecture with multimedia presentation.

N2. Laboratory: knowledge check in writing or oral form, report preparation, office hours.




concluding (at semester end)


achievement

Lecture PEK_W01, PEK_W02,

PEK_W03, PEK_W04

Writing exam

Laboratory

F1

PEK_U01, PEK_U02,

PEK_U03, PEK_U04,

PEK_U05

Laboratory preparation

F2 PEK_U01, PEK_U02,

PEK_U03, PEK_U04,

Laboratory activity

7

1

PEK_U05

F3 PEK_U01, PEK_U02,

PEK_U03, PEK_U04,

PEK_U05

Reports

P=0,3*F1+0,2*F2+0,5*F3


PRIMARY LITERATURE:

[39] Chwaleba A., Poniński M., Siedlecki A.: Metrologia elektryczna, WNT, Warszawa 2010.

[40] Tumański S.: Technika pomiarowa, WNT, Warszawa, 2007

[41] Kalus-Jęcek B., Wzorce wielkości elektrycznych i ocena niepewności pomiarów, Wyd.

Pol. Łódzkiej, Łódź, 2000

[42] Zajda Z., Żebrowski L., Urządzenia i układy automatyki PWr. Wrocław, 1993

[43] Miłek M., Metrologia elektryczna wielkości nieelektrycznych, Uniwersytet

Zielonogórski 2006.

[44] Janiczek R., Elektryczne miernictwo przemysłowe, Wydawnictwo Politechniki

Częstochowskiej 2006.

[45] Rząsa M., Kiczma B., Elektryczne i elektroniczne czujniki temperatury, WKŁ Warszawa

2005.

[46] Romer R., Miernictwo przemysłowe,wyd 3. PWN, Warszawa, 1978 [47] Wrocław 2001.


[1] Lisowski M., Podstawy metrologii, Of. Wyd. Pol. Wrocławskiej, Wrocław, 2011

[2] Piotrowski J., Podstawy miernictwa, WNT, 2003

[3] Stryburski W. Przetworniki tensometryczne – konstrukcja, projektowanie,

użytkowanie,WNT, Warszawa 1971.

[4] Minkinia W., Gryś S, Korekcja charakterystyk dynamicznych czujników

termometrycznych – metody, układy, algorytmy.

[5] www.czujniki.pl

[6] Editors: Erika Kress-Rogers and Christopher J. B. Brimelow - Instrumentation and

sensors for the food industry, second edition, CRC Press 2001

[7] Nestor 0. Shpak, Vadim P. Deynega Nikolay V. Kirianaki and Sergey Y. Yurish - Data

Acquisition And Signal Processing For Smart Sensors, John Wiley & Sons 2002


Daniel Dusza, [email protected]

http://www.czujniki.pl/

7

2


SUBJECT

Measurements in processing apparatus


Chemical Engineering

AND SPECIALIZATION …………………………….. Subject

educational

effect

Correlation between subject educational

effect and educational effects defined for

main field of study and specialization (if

applicable)**

Subject



number***

PEK_W01

(knowledge) K1Aic_W30 C1 Lec1 N1, N2

PEK_W02 K1Aic_W30 C1 Lec2, Lec3 N1, N2


Lec6, Lec7 N1, N2


Lec6, Lec7 N1, N2


Lec6, Lec7 N1, N2

PEK_U01

(skills) K1Aic_U16 C2 La1, La2, La3 N1, N2

PEK_U02 K1Aic_U16 C2 La4, La5,

La6, La7 N1, N2


La8, La9, La

10, La11,

La12, La13,

La14

N1, N2


La8, La9, La

10, La11,

La12, La13,

La14

N1, N2


La8, La9, La

10, La11,

La12, La13,

La14

N1, N2



7

3

Zał. nr 4 do ZW 64/2012


SUBJECT CARD

Name in Polish Metody badań materiałów

Name in English Methods of Materials Testing Main field of study (if applicable): Materials Engineering

Specialization (if applicable): Erasmus students


Kind of subject: obligatory / optional / university-wide*

Subject code ELR 021225

Group of courses YES / NO*


Number of hours of organized

classes in University (ZZU) 30

Number of hours of total student

workload (CNPS) 60


crediting with grade*

For group of courses mark (X) final

course

Number of ECTS points 2 including number of ECTS points for

practical (P) classes

including number of ECTS points for

direct teacher-student contact (BK)

classes

1

*delete as applicable PREREQUISITES RELATING TO KNOWLEDGE, SKILLS AND OTHER COMPETENCES

RELATING TO KNOWLEDGE:

1. Knowledge of advanced mathematics at the level permitting to understand mathematical problems in

engineering sciences.

2. Knowledge of the principles and laws of physics in the field of classic electrodynamics

(electrostatics, electricity, magnetostatics, electromagnetic induction, electromagnetic waves, optics)

and selected topics in physics: quantum, solid state, atomic nucleus.

RELATING TO SKILLS:

1. Ability of correct and effective application of advanced mathematics to qualitative and quantitative

analysis of mathematical problems related to the studied engineering discipline.

2. Ability of correct and effective application of the known principles and laws of physics for qualitative

and quantitative analysis of physical problems in the engineering.

SUBJECT OBJECTIVES C1. Acquiring a theoretically founded knowledge in the physical basics of the selected specialist

material diagnostic methods such as for example: electron microscopy, X-Ray diffraction, optical

methods, ultrasonic spectroscopy

C2. Acquiring knowledge in the qualitative and quantitative analysis of structural, optical and

electronic properties of solids

C3. Understanding the advanced methods of electrical quantities measurements, including the

electrostatic, as well as the magnetic ones in solids

C4. Acquiring the ability of organising tests and diagnostics of materials using the properly selected

7

4

methods



PEK_W01- Has the knowledge of X-Ray radiation properties and testing of crystalline materials

PEK_W02- Has the knowledge of light and electron beam interaction with a material

PEK_W03- Knows and understands the methods of material structure tests

PEK_W04- Has the knowledge of applying spectroscopy for material composition analysis

PEK_W05- Knows the principle of operation of atomic forces microscopes and tunnel microscopes

PEK_W06- Knows the possibilities of utilising the photoelectrons and Mössbauer spectrometry

PEK_W07- Has the knowledge of material resistance measurements and its dependence on external

factors

PEK_W08- Has the knowledge of manufacturing and properties of electrets

PEK_W09- Understands the role of dielectric spectroscopy methods in evaluation of the ageing

phenomena

PEK_W10- Has general knowledge of magnetic properties of solids

PEK_W11- Knows and understands the significance of ultrasounds in material diagnostics

PEK_W12- Has the knowledge of testing the mechanical and thermal properties of solids

PEK_W13- Knows the methods of testing thin films

relating to skills:

PEK_U01- Can independently determine parameters of selected materials

PEK_U02- Is able to interpret physical phenomena occurring during materials examination and testing

PEK_U03- Can utilise the known and properly selected methods for material diagnostics

PEK_U04- Is able to perform critical analysis of the obtained test results

PROGRAMME CONTENT

Form of classes - lecture Number

of hours

Lec 1 Scope of the lecture, literature, crediting conditions.

Structural X-Ray radiography 2

Lec 2 Light microscopy in materials testing 2

Lec 3 Electron microscopy. Preparation of specimens 2

Lec 4 Structural analysis using an electron beam 2

Lec 5 Qualitative and quantitative analysis of surface composition in solids 2

Lec 6 Atomic force microscopy 2

Lec 7 Determination of electron structure of solids. Photoelectron spectrometry.

Mössbauer spectrometry. 2

Lec 8, 9 Electrical properties of solids 4

Lec 10 Electrostatic properties tests of solids 2

Lec 11 Dielectric spectroscopy 2

Lec 12 Magnetic properties of solids 2

Lec 13 Ultrasounds in materials testing 2

Lec 14 Mechanical properties of solids and thermal tests of materials 2

Lec 15 Methodology of thin coverings and thin layers testing 2

Total hours 30

TEACHING TOOLS USED

N1. Traditional lecture accompanied by multimedia presentation and discussion

N2. Own work of a student

N3. Office hours

N4. Short quizzes before lab classes

N5. Report preparation.

7

5





end)

Educational effect


Wykład

P1 PEK_W01

PEK_W13

Written examination

Laboratorium

F1

F2

PEK_U01 PEK_U04

Quiz /oral answer Report from the laboratory exercises

P2= α1 F1+ α2F2 = 0,5 F1 + 0,5 F2


PRIMARY LITERATURE:

[1] Newell J., Essentials of modern materials science and engineering, John Wiley and Sons, Inc. 2009

[2] Celiński Z., Materiałoznawstwo elektrotechniczne, Oficyna Wydawnicza Politechniki

Warszawskiej, Warszawa, 2011

[3] Szuber J. Powierzchniowe metody badawcze w nanotechnologii półprzewodnikowej,

Wydawnictwo Polit. Śląskiej, Gliwice 2002

[4] Briggs D., Seah M. P., Auger and X-ray photoelectron spectroscopy, Vol. I, II, John Willey and

Sons Ltd. 1990

[5] Lyman Ch. E., Goldstein J. I., Scanning electron microscopy, X-ray microanalysis and analytical

electron microscopy. A laboratory workbook. Premium Press, New York and London, 1990


[1] Hummel Rolf, Electronic properties of materials, Springer-Verlag, NewYork, 1985

[2] Oleś A., Metody doświadczalne fizyki ciała stałego, WNT, Warszawa, 1998

[3] Recent papers on methods of materials testing


Bożena Łowkis [email protected]


7

6


FOR SUBJECT

Methods of Materials Testing

AND EDUCATIONAL EFFECTS FOR MAIN FIELD

OF STUDY Materials Engineering AND SPECIALIZATION ……………………………..



effects defined for main field of

study and specialization (if

applicable)**

Subject



number***

PEK_W01 (knowledge) K1Aim _W21 C1. Wy 1 N1.- N3.

PEK_W02,

PEK_W03

K1Aim _W21 C1., C2. Wy 2, 3, 4 N1.-N3.

PEK_W04 K1Aim _W21 C2. Wy 5 N1.-N3.

PEK_W05 K1Aim _W21 C2. Wy 6 N1.-N3.

PEK_W06 K1Aim _W21 C1., C2. Wy 7 N1.-N3.

PEK_W07 K1Aim _W21 C3. Wy 8,9 N1.-N3.

PEK_W08 K1Aim _W21 C3. Wy 10 N1.-N3.

PEK_W09 K1Aim _W21 C3. Wy 11 N1.-N3.

PEK_W10 K1Aim _W21 C3. Wy 12 N1.-N3.

PEK_W11 K1Aim _W21 C1. Wy 13 N1.-N3.

PEK_W12 K1Aim _W21 C2. Wy 14 N1.-N3.

PEK_W13 K1Aim _W21 C2. Wy15 N1.-N3.

PEK_U01 (skills) K1Aim_U24 C4. La1La10 N4.-N5.

PEK_U02 K1Aim_U24 C4. La1La10 N4.-N5.





7

7

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Mikrobiologia II

Name in English Microbiology II Main field of study (if applicable) Biotechnology




Subject code BLC013004



Number of hours of






/ crediting

with grade*

Examination

/ crediting

with grade*

Examination

/ crediting

with grade*

Examination

/ crediting

with grade*

Examination

/ crediting


(X) final course

Number of ECTS points 3 2 including number of ECTS




student contact (BK) classes 1 1.5



COMPETENCES

29. Higher school level of biology.

30. Microbiology fundamentals

SUBJECT OBJECTIVES

C1 Cognoscense of bacterial genetics.

C2 Cognoscense of bacterial metabolisms.

C3 Cognocsense of the physical-chemical factors influencing bacterial metabolism.

C4 Cognoscense of the elaboration and realization of the experiments with the microbes

- individually.

7

8



Person who finish the course:

PEK_W01 – knows the rules of DNA replication in prokaryotic cells and is able to

characterize the bacterial cell cycle and is able to point the reasons of

differentiation in bacterial populations.

PEK_W02 – knows the path of protein synthesis and modification in bacterial cells

PEK_W03 – knows the bacterial metabolic pathways

Relating to skills:

Person who finish the course:

PEK_U01 - is able to evaluate the influence of physical and chemical factors on the

bacterial growth

PEK_U02 – is able to plan and make the experiments form the area of general microbiology

Relating to social competences: PEK_K01

PEK_K02

…

PROGRAMME CONTENT


Lec 1 Bacterial genetics. DNA replication, plasmids characteristic. 2

Lec 2 Bacterial genetics. Variability in bacterial cells: DNA transfers –

transformation, transduction, coniugation. 2

Lec 3 Bacterial genetics. Mutagenesis, SOS mechanism. 2

Lec 4

Lec 5

Bacterial genetics. Division of the bacterial cell, bacterial colonies

formation (aggregation). Protein synthesis and the control of genes

expression – operons.

2+2

Lec 6

Lec 7

Bacterial life cycles. Different bacterial spores. Endospore growing

(Baccilus sp. and Clostridium sp.) 2+2

Lec 8 Bacterial metabolism. Hexoses catabolism (organic donors of

reductive equivalents): glycolysis, KDPG and pentoses cycles (split

C6 into C3). Introduction into further metabolic pathways using C3

molecules (aerobic and anaerobic respiration; anaerobic and aerobic

fermentations).

2

Lec 9 Bacterial metabolism. Aerobic metabolism – aerobic respiration,

Crebs cycle, anaplerotic pathways (glioxalic cycle), reductive

equivalents synthesis. Structure, location and function of redox

chain – electron transfer system; ATP restoration. Oxygen as a final

electrons acceptor coming from the redox chain.

2

Lec 10 Bacterial metabolism. Anaerobic metabolism. Aerobic and

anaerobic respiration – comparison. Representative examples of

anaerobic respiration: nitrate, sulphate, phosphate respirations.

Mechanism of reduction of final acceptors reduction by electrons

coming from the redox chain (anabolic and catabolic).

2

7

9

2

Lec 11 Bacterial metabolism. Anaerobic metabolism – fermentations:

alcohol, lactic, propionic, butyric. ATP synthesis – acetylphosphate

as a phosphorus donor. Oxygenic fermentations – metabolic

pathways leading to carboxylic acids and keto acids.

2

Lec 12 Bacterial metabolism. Inorganic sources of reductive equivalents –

electron transfer under anaerobic conditions. Reverse electron

transfer – NADH and NADPH obtaining. Assimilation of carbon

dioxide: Calvin cycle, reductive TCC cycle, reductive acetyl-CoA

pathway. Methanogenes and methylotrphs characteristic.

2

Lec 13 Bacterial metabolism. Photosynthetic bacterial species: chlorophylls

and photosystems structures. Oxygenic and anoxygenic

photosynthesis. Basics of bacterial systematics.

2

Lec 14 Final test – I approach 2

Lec 15 Final test – II approach 2

Total hours 30


Cl 1

Cl 2

Cl 3

Cl 4

…

Total hours


Lab 1 Rules of lab credits. Rules of safety and work in microbial lab. 3

Lab 2 Nutrition requirements of bacteria I. Inoculation of bacteria on minimal

and complete media – intensity of growth observation and comparison

of different bacterial colonies. Inoculation of chosen bacterial strains on

media with different nitrogen and carbon sources. Growth observations

– optimal composition of cultivation media for particular bacterial

strains.

3

Lab 3 Nutrition requirements of bacteria II. Inoculation of bacteria on minimal

and complete media – intensity of growth observation and comparison

of different bacterial colonies. Inoculation of chosen bacterial strains on

media with different nitrogen and carbon sources. Growth observations

– optimal composition of cultivation media for particular bacterial

strains.

3

Lab 4 The influence of physic factors on bacterial growth I. Optimal

temperature of growth of chosen bacterial strains. Thermal lethal point

assignment; influence of drying on the bacterial growth. 3

Lab 5 The influence of physic factors on bacterial growth II. Thermal lethal

time assignment for chosen strains. The influence of UV radiation on the

bacterial strains growth. 3

Lab 6 The influence of chemical factors on bacterial growth. Optimal pH of

growth assignment for chosen strains. The influence of disinfectants on

the growth of chosen strains. 3

8

0

Lab 7 Fundamentals of bacterial diagnostics – Gram staining. 3

Lab 8 Antibiotics resistant I: Applied methods of evaluation. 3

Lab 9 Antibiotics resistant II: application of chosen drugs. 3

Lab 10 Bacterial metabolism I: sugars fermentation. 3

Lab 11 Bacterial metabolism II: nitrogen metabolism, assessment of the activity

of the exogenous bacterial enzymes. 3

Lab 12 Fundamentals of yeasts cultivation and viability evaluation. 3

Lab 13 Checking the results of previous experiments. Lab for students with

absences, allowing completing the missing subjects. 3

Lab 14 Credit – first attempt. Experimental and theoretical part. 3

Lab 15 Credit – second attempt. Experimental and theoretical part. 3

Total hours 45


Proj 1

Proj 2

Proj 3

Proj 4

…

Total hours

Form of classes - seminar Number of hours

Sem 1

Sem 2

Sem 3

Sem 4

…

Total hours

TEACHING TOOLS USED


N2 Individual laboratory work

…


Evaluation


semester),


semester end)

Educational effect


achievement

C (lecture) PEK_W01-

PEK_W03

Final test

C (laboratory) PEK_U01 – Final test

8

1

U02PEK_U02


PRIMARY LITERATURE:

[48] P. Ketchum et all „Microbiology – Concepts and applications”

[49] Michael T. Madigan et all “Biology of Microorganisms”

[50] „Mikrobiologia” ; H.G. Schlegel


[1] „Życie bakterii” W. Kunicki-Goldfinger,

[2] „Bakterie w biologii, biotechnologii i medycynie” P. Singleton,

SUBJECT SUPERVISOR


Dr hab. Ewa Żymańczyk-Duda, prof. Pwr, [email protected]


FOR SUBJECT

Microbiology II


Biotechnology

Subject

educational

effect





Subject



number***

(knowledge)

PEK_W01 K1Abt_W17 C1 Wy1-Wy3 N1

PEK_W02 K1Abt_W17 C1 Wy4- Wy7 N1

PEK_W03 K1Abt_W17 C2 Wy8-Wy13 N1

…

(skills)

PEK_U01 K1Abt_U16 C3,C4 La1-La13 N2

PEK_U02 K1Abt_U16 C3,C4 La14-La15 N2



8

2

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Chemia organiczna

Name in English Organic chemistry Main field of study (if applicable) chemia


Level and form of studies: 1st/ full-time





Number of hours of


University (ZZU) 30



Form of crediting /crediting

with grade


(X) final course





student contact (BK) classes 0.5



COMPETENCES

1. Chemistry on secondary school level.

2. Mathematic on secondary school level.

3. Captured knowledge of "Fundamentals of Organic Chemistry"

4. Mastered the basic steps and laboratory techniques

5. Mastered skill calculations based on the reaction of stoichiometric equations

SUBJECT OBJECTIVES

C1 To familiarize students with the basic terminology, chemical symbols, types of

bonds, and the classification of the reaction.

C2 To familiarize students with the organic molecules building (hybridization,

isomerism)

C3 Basic knowledge about the properties and reactivity of different groups of organic

compounds

C4 To familiarize students with the basic organic reaction mechanisms: radical and

8

3

electrophilic addition, nucleophilic and electrophilic substitution, elimination, aldol

condensation, esterification hydrolysis, acylation, ester-type condensation, Michael

addition

C5 Fundamentals of analysis of organic compounds: chemical identification and

spectroscopic methods

C6 Learning self-solve issues and problems related to the reactivity of organic

compounds, reactant planning, anticipation of the reaction products

C7 To familiarize students with more advanced experimental techniques in organic

synthesis

C8 Get to know the different types of functional group transformations and methods of

carbon skeleton construction (the synthesis of various products)

C9 Learn to use the chemical literature (issue of encyclopedic and original papers) and

searchable databases

C10 Preparing students to perform simple synthesis and identification of organic

compounds



PEK_W01 – Can correctly classify and name the basic groups of organic compounds

PEK_W02 – It can analyze the problems of the structure and isomerism of organic

compounds

PEK_W04 – Can describe the chemical properties of the different groups of compounds

PEK_W05 – Understand the basic types of reaction (mechanisms)

PEK_W06 – familiar with more advanced experimental techniques used in organic

chemistry: different types of distillation (simple, azeotropic, steam, under

reduced pressure), chromatography.

PEK_W07 – understands how each type of reaction can modify the structure

PEK_W08 – know the basic types of reactants (oxidants, reducers, nukleofile, dehydrating

agent, a nitrating mixture)

Relating to skills:

PEK_U01 – Knows how to predict products of basic reaction

PEK_U02 – Can plan the synthesis of simple organic compound

PEK_U03 – Can identify simple compounds using chemical and/or spectroscopic methods

PEK_U04 – knows how to build the apparatus required for experiment

PEK_U05 – knows how to purify and identify the reaction products

PEK_U06 – know how to search the literature to find a recipe and properties specified

products

PEK_U07 – know how to document the process and the results of experiments (calculations

and measurements)


La1

How the classes will be conducted and evaluated; safety rules in the

chemical laboratory; familiarizationwith the equipment (laboratory

cabinets)

2

La2 Oxidation and reduction reactions; conducting an experiment of

oxidation o reduction (for assistant choice)

4

La3 Nucleophilic substitution reaction 4

La4 Elimination reaction – dehydratation 4

8

4

La5 Addition reaction to carbonyl group 4

La6 Electrophilic substitution in aromatic ring 4

La7 Cycloaddition – Diels-Alder reaction 4

La8 Separation organic compounds from natural sources and

identification.

4

Total hours 30

TEACHING TOOLS USED

N1 Overview of the issues

N2 discussion how to understand/solve problems

N3 solving problems

N4 accurate explanation of the planned experiment

N5 Individual (or in pairs) condudtion of the 6 experiments proposed by Assistant and

the isolation of 1 product of natural origin

N6 detailed documentation of experiments- keeping notes (lab reports)


Evaluation


semester),


semester end)

Educational effect


achievement

F1(classes) PEK_W01 –

PEK_W05

PEK_U01

Test I (min 50%)

F2(classes) PEK_W01 –

PEK_W05

PEK_U02

PEK_U03

Test II (min 50%)

F1 (laboratory) PEK_W06-

PEK_W08

Partial test

F2 (laboratory) PEK_U02,

PEK_U04-

PEK_U07

evaluation on the basis of the preparation,

the performation and documentation of all

experiments

C (classes) = 3,0 when (F1 + F2)/2 = 50-60%

3,5 when (F1 + F2)/2 = 61-70%

4,0 when (F1 + F2)/2 = 71-80%

4,5 when (F1 + F2)/2 = 81-90%

5,0 when (F1 + F2)/2 = 91-97%

5,5 when (F1 + F2)/2= 98-100%

C (laboratory) = (F1 + F2)/2

8

5


PRIMARY LITERATURE:

[51] Exercises and problems to solve published/available in the Internet.

[52] P. Mastalerz, Chemia organiczna, PWN, Warszawa, 1986.

[53] A. Zwierzak, Zwiezły kurs chemii organicznej, tom I i II, Wydawnictwo Politechniki

Łódzkiej, Łódz, 2000, 2002.

[54] L. Achremowicz, M. Soroka, Chemia organiczna. Laboratorium, Skrypt Politechniki

Wrocławskiej, Wrocław, 1980. Wersja elektroniczna: e-książki, www.bg.pwr.wroc.pl

[55] L. Achremowicz, Laboratorium chemiczne, Skrypt Politechniki Wrocławskiej,

Wrocław, 1994

[56] A. I. Vogel, Preparatyka organiczna, WNT, Warszawa, 2006


[33] J. McMurry, Chemia organiczna, tom 1-5, PWN, Warszawa 2005.

[34] D. Buza, W. Sas, P. Szczecinski, Chemia organiczna. Kurs podstawowy, Oficyna

Wydawnicza Politechniki Warszawskiej, Warszawa, 2006.

[35] chemical databases available online

SUBJECT SUPERVISOR


Dr inż. Renata Siedlecka, [email protected]


FOR SUBJECT

…………Organic Chemistry……………….


…………Chemistry, Biotechnology……………….

Subject

educational

effect





Subject



number***

(knowlwdge)

PEK_W01

K1Ach_W07

K1Ach_U26 C1 Cl1, Cl3 N1, N2, N3

PEK_W02 K1Ach_W07

K1Ach_U26 C2 Cl2 - Cl7 N1, N2, N3

PEK_W04 K1Ach_W07

K1Ach_U26 C3

Cl3 – Cl9

Cl12 – Cl14 N1, N2, N3

PEK_W05 K1Ach_W07

K1Ach_U26 C4

Cl3, Cl4, Cl6,

Cl9, Cl10, Cl11 N1, N2, N3

PEK_W06 K1Abt_U18 C7-C10 L2-L8 N4-N6



(skills)

PEK_U01

K1Ach_W07

K1Ach_U26 C6 Cl3 – Cl14 N1, N2, N3

8

6

PEK_U02

K1Ach_W07

K1Ach_U26

K1Abt_U18

C6

C7-C10

Cl3 – Cl13

L2-L8

N1, N2, N3

N4-N6

PEK_U03 K1Ach_W07

K1Ach_U26 C5 Cl3 – Cl13 N1, N2, N3

PEK_U04 K1Abt_U18 C7-C10 L2-L8 N4-N6






8

7

Zał. nr 4 do ZW 33/2012

FACULTY OF CHEMISTRY / DEPARTMENT OF CHEMICAL AND BIOCHEMICAL

PROCESSED

SUBJECT CARD

Name in Polish: Fizykochemiczne podstawy inżynierii procesowej

Name in English Physico-chemical bases of process

engineering Main field of study (if applicable):

Specialization (if applicable):

Level and form of studies: 2nd level, full-time

Kind of subject:: obligatory

Subject code: ICC014004

Group of courses: No

*delete if not related


Number of hours of





Form of crediting Exam

Credited

with grade

Credited

with grade


(X) final course





student contact (BK) classes 1.5 1 1

* delete if not related


COMPETENCES

31. Calculations of dervatives

32. Understanding of basic physics laws

SUBJECT OBJECTIVES

C1 To obtain knowledge about phase equilibria description

C2 To obtain knowledge of numerical solutions of thermodynamics problems

8

8


The scope of knowledge:

The person who completed the course:

PEK_W01 – is familiar with the essential notions of thermodynamics, particularly in the

context of thermodynamic transformations

PEK_W02 – is familiar with the essential notions of fluid thermodynamics

PEK_W03 - is familiar with the methods of thermodynamic characterization of pure and

mixed system using the phase diagrams

PEK_W04 - is familiar with the essential notions of phase transitions

PEK_W05 – knows the way of characterization of pure substances

PEK_W06 – knows the idea and the goal of distinction between ideal and real systems

PEK_W07 –can characterize qualitatively and quantitatively equilibrium conditions in

multicomponent systems

The range of skills:


PEK_U01 – is able to calculate properties of pure and mixed systems using the equation of

state

PEK_U02 - is able to solve problems related to phase equilibria

PEK_U03 - is able to determine the thermodynamic properties

PEK_U04 – is able to design experiments to determine phase equilibrium

PEK_U05 – is able to conduct the experiments, to interpret the obtained results and state the

conclusions

The social expertise:


PEK_K01 – is able to cooperate and work with the others in one team

PROGRAMME CONTENT

Form of classes - lecture Number of

hours

Le1 Introduction to the topic of the lecture. Basic thermodynamic

definitions 2

Le2 Methodology of saturated pressure determination 4

Le3 Equations of state. 2

Le4 Equations of Van der Waals type 4

Le5 Humid gases, equation of Molier 3

Le6 Solutions, basic notions. Ideal solution. Equation Gibbs – Duhem 6

Le7 Partial quantities. Notion of fugacity 3

Le8 Phase equilibria in multicomponent systems 3

Le9 Special cases of phase equilibria: distillation, absorption, extraction 3

Total hours 30

8

9

Form of classes - excercises Number of

hours

Ex1 Introduction and methodology 2

Ex2 Problems related to equation of state 2

Ex 3 Partial exam1 2

Ex 4 Problems related to thermodynamic properties of pure systems 2

Ex 5 Problems related to thermodynamic properties of solutions 4

Ex 6 Problems related to phase equilibria in multicomponent systems 4

Ex 7 Partial exam 2 2

Ex 8 Final exam 2

Total hours 30

Form of classes – laboratory Number of

hours

L1 Basic rules of work in laboratory. Orderliness of the classes. 2

L2 Laboratory exercises of determination of the basic thermodynamic

parameters. 8

L3 Laboratory exercises of diffusivity processes. 4

L4 Laboratory exercises of heat transfer processes. 8

L5 Laboratory exercises of phase equilibria processes. 8

Total hours 30

TEACHING TOOLS USED

N1 Lecture

N2 Problem sessions

N3 Laboratory experiment





end)


achievement

P (lecture) PEK_W01-W09 Final exam

F1 PEK_U01 –U02 Partial evaluation 1

F2 PEK_U02 –PEK_U03 Partial evaluation 2

F3 PEK_U01 –PEK_U03 Activity during the sessions

F4 PEK_U01 –PEK_U03 Absence – not excused

grade = 3,0 if (F1 + F2 + F3 + F4) = 100 – 120 pts.

3,5 if (F1 + F2 + F3 + F4) = 121 – 140 pts.

4,0 if (F1 + F2 + F3 + F4) = 141 – 160 pts.

4,5 if (F1 + F2 + F3 + F4) = 161 – 180 pts.

5,0 if (F1 + F2 + F3 + F4) = 181 – 200 pts..

5,5 if (F1 + F2 + F3 + F4) = 201 – pts.

P (laboratory) PEK_U05, Conducting of all laboratory exercises, to

9

0

PEK_K01 account for the all laboratory reports,

theoretical preparation to the each class.


PRIMARY LITERATURE [57] B.Kuchta, lecture copies, Internet (address will be given)

[58] S. Michałowski, K. Wańkowicz, Termodynamika procesowa, WNT, Warszawa, 1999

[59] J. M. Smith, H. C. Van Ness, M. M. Abbot, Introduction to Chemical Engineering

Thermodynamics, MCGraw Hill, Boston 2001.


[36] R. Koch, A. Kozioł, Dyfuzyjno – cieplny rozdział substancji, WNT, Warszawa, 1999

[2] S. R. Turns, Thermodynamics. Concepts and Applications, Cambridge University

Press, Cambridge 2006


Prof. dr hab. inż. Bogdan Kuchta

[email protected]

MATRIX OF CORRELATION BETWEEN EDUCATIONAL EFFECTS FOR SUBJECT

Physico-chemical bases of process engineering

AND EDUCATIONAL EFFECTS FOR MAIN FIELD OF STUDY Chemical engineering

Subject

educational

effect

Correlation between subject educational

effect and educational effects defined

for main field of study and


Subject

objectives***

Programme

content***

Teaching tool

number***

(knowledge)

PEK_W01

K2Aic_W06 C1 Le1, Le 2 N1

PEK_W02 K2Aic_W06 C1 Le 2 N1

PEK_W03 K2Aic_W06 C1 Le 3 – Le 5 N1

PEK_W04 K2Aic_W06 C1 Le 3- Le 4 N1

PEK_W05 K2Aic_W06 C1 Le 3 – Le 7 N1

PEK_W06 K2Aic_W06

C1 Le 3 – Le 4

Le7 N1

PEK_W07 C1 Le 6 – Le 9 N1

(skills)

PEK_U01 K2Aic_W06 C2 Ex1 – Ex2 N2

PEK_U02 K2Aic_W06 C2 Ex 3 – Ex 5 N2

PEK_U03 K2Aic_W06 C2 Ex 6 – Ex 8 N2

PEK_U05 K1Aic_U13 C2 L1 – L5 N3

(social

expertise)

PEK_K01

K1Aic_U13 C2 L1 – L5 N3



9

1

Zał. nr 4 do ZW 33/2012

WROCLAW UNIVERSITY OF TECHNOLOGY

DEPARTMENT OF CHEMISTRY

DESCRIPTION OF THE COURSES

Polish name Recykling materiałów

English name Recycling of materials Field of study (if applicable): Materials Engineering

Speciality (if applicable): Erasmus students

Form of the course completion: 1. degree, stationary

Type of course: obligatory

Course code IMC024009

Group of courses YES


Number of

hours/semester (ZZU) 30

Total Student’s Workload

(CNPS) 30

Form of the course

completion

credit with

a

grade/test

For a group of courses,

select the final course (X)

ECTS credits 2

Number of practical

hours (P)

including the number of

credits corresponding to

the classes requiring

direct contact (BK)

1

REQUIREMENTS FOR KNOWLEDGE, SKILLS AND OTHER COMPETENCE

1. General Chemistry

COURSE OBJECTIVES

C1 To familiarize students with the basic terminology of waste

C2 To familiarize students with the structure and systems of waste collection.

C3 To familiarize students with the basic methods of waste management.

C4 Awakening of environmental awareness.

9

2

PARTICULAR LECTURE CONTENT

In the field of knowledge:

A person who has passed the examination:

PEK_W01 – Student knows the basic terminology associated with waste management.

PEK_W02 – Student has a basic knowledge about the symbols and designations used to

label the materials for recycling.

PEK_W03 – Student has a basic knowledge of the collection and distribution systems of

waste materials.

PEK_W04 – Knows the basic legal conditions for recycled materials.

…

In a field of social skills:

A person who has passed the examination:

PEK_K01 – is aware of the risks arising from poor waste management.

Course Content

Form of teaching - lecture hours

Wy1

Selective collection systems. The division, the definition and sources

of municipal waste and hazardous waste. Principles of waste

management, basic definitions related to waste management.

Logistics, waste recycling, its advantages and disadvantages,

problems. Examples.

2

Wy2

Classification, labeling materials. The overall breakdown of

characters and graphic symbols used to mark the packaging,

recycling signs, signs indicating the proper waste handling.

2

Wy3

Waste management in Poland, part 1: Material Recycling -

definition, elements of the system, the barriers in the recycling

process, the criteria for suitability for recycling.

2

Wy4

Waste management in Poland, part 2: Material recycling -

European standards (applicable in Poland), heavy metals in the raw

materials from recycling, recycling of paper and cardboard, recycling

of glass packaging, metal packaging recycling, recycling of timber

packaging and multimaterial packaging.

2

Wy5 Waste management in Poland, part 3: Material recycling -

recycling of plastic packaging. 2

Wy6

Waste management in Poland, part 4 Feedstock recycling -

definition, criteria for suitability for recycling of raw materials,

disadvantages, advantages. Thermal and solvolytic processes used in

the recycling of raw materials, examples.

2

Wy7

Biological treatment part 1: Composting. The legal basis,

advantages and disadvantages, the criteria for the use of composting,

limitations and conditions of composting, discuss progress and

process parameters (pH, temperature, microorganisms).

2

Wy8

Biological treatment, part 2: Methane fermentation. Definition,

classification, advantages, disadvantages, differences between

composting and fermentation, fermentation steps, the most important

parameters and microorganisms involved in the fermentation process.

Fermentation methods one and two-stage, advantages and

2

9

3

disadvantages. The substrates and products.

Wy9 Incineration of waste. Basic problems of waste incineration plants,

safety, advantages and disadvantages. 2

Wy10

Hazardous waste, part 1 - Definition, classification, origin.

Methods of dealing with pharmaceuticals, batteries, fluorescent

lamps, mercury-containing waste, appliances containing freon,

electronics.

2

Wy11 Hazardous waste, part 2 - Legislation. Disposal of used oils.

Proceedings of vehicles spent product. 2

Wy12 Analysis of the life cycle of consumables. For selected examples -

production, operation, recovery (home appliances, AGD). 2

Wy13 Waste management in selected countries. 2

Wy14 Efforts to improve the situation in the field of waste

management. Shares information and education, legal, collection

and transport, recovery, disposal.

2

Wy15 Ethical problems related to the production and consumption. 2

Total hours 30

TOOLS FOR TEACHING


N2 discourse

PERFORMANCE EVALUATION OF THE EFFECTS OF EDUCATION

Notes (F – formująca

(w trakcie semestru), P

– podsumowująca (na

koniec semestru))

Number of the

effect of education

How to assess the achievement of the effect

of education

P (lecture) PEK_W01-

PEK_W04

test

BASIC AND SUPPLEMENTARY LITERATURE

BASIC LITERATURE:

[60] Systemy recyklingu odpadów opakowaniowych w aspekcie wymagań

ochrony środowiska / Hanna Żakowska, Wydawnictwo Akademii Ekonomicznej,

2008

[61] Odpady komunalne: zbiórka, recykling, unieszkodliwianie odpadów

komunalnych i komunalnopodobnych, Wydawnictwo Politechniki Krakowskiej,

2005

[62] Procesy logistyczne w gospodarce odpadami / Józef Bendkowski, Maria

Wengierek, Wydawnictwo Politechniki Śląskiej, 2002

SUPPLEMENTARY LITERATURE:

9

4

[63] Odzysk ciepła w procesie termicznej utylizacji odpadów medycznych /

Janusz Wojciech Bujak, oficyna Wyd.Politechniki Wrocławskiej, 2010

[64] Wybrane zagadnienia recyklingu samochodów, Jerzy Osiński, Piotr Żach,

Wydawnictwa Komunikacji i Łączności, 2006

COURSE SUPERVISOR

(title, name, surname, e-mail adress)

Dr inż. Konrad Szustakiewicz, [email protected]

MATRIX RELATION TO EFFECTS OF EDUCATION COURSE

Recycling of Materials

The EFFECTS OF EDUCATION IN THE SPECIALIZATION

Inżynieria materiałowa

Particular

lecture

content

reference to the effect of the

learning outcomes defined for

the field of study and

specializations (if applicable)**

Course

objectives

***

Course

Content

***

Tools for

teaching ***

(knowledge)

PEK_W01 K1Aim _W33 C1, C2 Wy1, Wy2 N1

PEK_W02 K1Aim _W33 C1, C2 Wy1, Wy1, N1

PEK_W03 K1Aim _W33 C2, C3 Wy3-Wy14 N1

PEK_W04 K1Aim _W33 C1, C2, C3, Wy3-Wy14 N1

PEK_K01 K1Aim _W33 C4 Wy15 N2

** - wpisać symbole kierunkowych / specjalnościowych efektów kształcenia

*** - odpowiednie symbole z tabel powyżej

9

5

Zał. nr 4 do ZW 64/2012



SUBJECT CARD

Name in Polish Grafika inżynierska

Name in English Technical drawing Main field of study (if applicable) all fields of study


Level and form of studies: 1st/2nd level, full-time


Subject code GFC011002



Number of hours of


University (ZZU) 30




/ crediting

with grade*

Examination

/ crediting

with grade*

crediting

with grade Examination

/ crediting

with grade*

Examination

/ crediting


(X) final course









COMPETENCES

33. Basic knowledge of computers

SUBJECT OBJECTIVES

C1 Familiarisation with the technical drawing conventions.

C2 Learning of reading and making a design drawing.

C3 Working knowledge of using the computer aided design software in making and

modifying the technical documentation.

9

6


Relating to skills:

PEK_U01 – understands the conventions of technical drawing and the role of

standardization on technical drafting.

PEK_U02 – can project the planar and three-dimensional objects in views.

PEK_U03 – possesses skills at representation and dimensioning of existing and proposing

objects according to technical drawing conventions.

PEK_U04 – has the sufficient knowledge of reading the design drawings and chemical plant

diagrams.

PEK_U05 – has the working knowledge of using the computer aided design applications in

making the technical documentation.

PROGRAMME CONTENT


Lab 1 Organising class. Familiarisation with the safety rules in the

computer room. Teaching tools and conditions of course credition.

Introduction to CAD application – user interface, workspace,

drawing area, creating and modifying of objects in AutoCAD.

2

Lab 2 Conventions of technical drawing (types of drawing, drawing sizes,

scales, title blocks, line styles and types, technical lettering).

Settings of parameters in AutoCAD (layer management, setting of

attributes, co-ordinate systems).

2

Lab 3 Standardization on technical drawing. Polish Committee for

Standardization and it’s normalization activity. Searching for

standards exercises. Drawing objects in AutoCAD: line, polyline,

arc, circle, ellipse, rectangle, poligon.

2

Lab 4 Representation of 2D and 3D objects (axonometric, orthographic

and perspective projections). Selection and modifications of objects

in AutoCAD: move, copy, rotate, mirror, scale, trim, extend, break,

fillet, chamfer, explode, offset.

2

Lab 5 Representation of the internal structural details of object. Sections

types: one and more cutting planes, revolved, removed, local,

developing. Basic conventions of sections and cuts. Long objects -

interrupted views. Symmetrical and revolving objects –

representation conventions.

2

Lab 6 Dimensioning on technical drawing (indications, graphic form,

rules). Printing of technical documentation in AutoCAD. 2

Lab 7 Repetition and test I. 2

Lab 8 Sectioning of 3D objects. Representation of interpenetrating solids.

Curve of interpenatration. 2

Lab 9 Representations and dimensioning of tapers and slopes. 2

Lab 10 Types of joints in engineering constructions. Representation,

designation and dimensioning of assembled threaded parts and

selected inseparated joints. Simplified representation and

dimensioning on technical drawing.

2

Lab 11 Tolerance of dimensions, fitting of elements, deviations of shape, 2

9

7

position and surface finish specifications. Lab 12 Design drawing (assembly and production drawings). 2

Lab 13 Diagram drawing. Graphical symbols for diagrams. Chemical

equipment representation on diagram. Process flow diagrams for

chemical industry.

2

Lab 14 Test II 2

Lab 15 Correction test. Course acceptance. 2

Total hours 30

TEACHING TOOLS USED

N1 Multimedia presentations

N2 Using of AutoCAD software


Evaluation


semester),


semester end)

Educational effect


achievement

F1 PEK_U01-

PEK_U02

test I

F2 PEK_U03-

PEK_U06

test II

F3-F8 PEK_U02-

PEK_U06

drawings made in AutoCAD

C=[(F1+F2)/2+(F3+F4+...+F8)/6]/2

3,0 if 3,25 < C

3,5 if 3,25 C< 3,75

4,0 if 3,75 C < 4,25

4,5 if 4,25 C < 4,75

5,0 if 4,75 C

9

8


PRIMARY LITERATURE:

[65] Dobrzański T.: Rysunek techniczny maszynowy, WNT, Warszawa 2010.

[66] Pikoń A.: AutoCAD 2011. Pierwsze kroki, Helion, 2011.


[37] Burcan J.: Podstawy rysunku technicznego, WNT, 2010.

[38] Jaskulski A.: AutoCAD 2011/LT2011+ kurs projektowania parametrycznego i

nieparametrycznego 2D i 3D: wersja polska i angielska, Wydawnictwo Naukowe

PWN, 2010 (PWr on-line library).

SUBJECT SUPERVISOR


Dr inż. Izabela Polowczyk, [email protected]


FOR SUBJECT

Technical drawing


(All fields of study at the Faculty of Chemistry)

Subject

educational

effect





Subject



number***

(competences)\

PEK_U01

K1Aim_U13, K1Ach_U39,

K1Aic_U13, K1Atc_U38, K1Aim_U13 C1 Lab1-Lab3 N1

PEK_U02 K1Aim_U13, K1Ach_U39,

K1Aic_U13, K1Atc_U38, K1Aim_U13 C2 Lab4-Lab5 N1, N2






K1Aic_U13, K1Atc_U38, K1Aim_U13 C3 Lab1-Lab15 N2



9

9

Zał. nr 4 do ZW 64/2012

FACULTY of CHEMISTRY / DEPARTMENT………………

SUBJECT CARD

Name in Polish Bezpieczeństwo techniczne

Name in English Technical safety Main field of study (if applicable): Chemical Technology

Specialization (if applicable): ……………………..


Kind of subject: obligatory / optional / university-wide*


Group of courses YES / NO*


Number of hours of


University (ZZU)

15 15

Number of hours of

total student workload

(CNPS)

30 30


crediting with

grade*

Examination /

crediting with

grade*

Examination /

crediting with

grade*

Examination /

crediting with

grade*

Examination /

crediting with

grade*

For group of courses

mark (X) final course

Number of ECTS points 1 1 including number of

ECTS points for practical

(P) classes

1

including number of

ECTS points for direct

teacher-student contact

(BK) classes

1 1



1. Knowledge of chemistry on the secondary school level

2. Fundamental knowledge on the chemical safety

3. Skill in computer operation \

SUBJECT OBJECTIVES C1 To familiarize students with the basics of technical safety C2 National and European law regulations related to the technical safety

C3 Learning algorithms for analysis of industrial installations hazards

C4 Teach students of the health risk assessment associated with industrial failures

C5 Familiarizing students with examples of spreading chemical pollution and with the

methodology of calculations of spreading the contaminants in the environment

1

0

0



PEK_W01 - familiar with basic concepts and definitions of technical safety

PEK_W02 - can specify the basic legislative acts governing the national and European

technical safety rules

PEK_W03 – knows the common elements of industrial operational and emergency response

PEK_W04 – familiar with the main provisions of environmental law, Seveso III directive and

of the Convention on the transboundary effects of industrial accidents

PEK_W05 – able to apply methods of risk analysis to identify possible failure in industrial

installations

PEK_W06 – knows how to describe the basic methods of analysis of the health risks in areas

contaminated as a result of industrial accidents

relating to skills:

PEK_U01 – can use the databases in order to classify plants in terms of the risks involved

PEK_U02 – knows how to carry out an analysis of the hazards in simple industrial installations

PEK_U03 – can suggest remedial measures in the event of an industrial accident in simple

chemical installations

PEK_U04 – can perform simple calculations of exposure to the contamination of the

environment after the failure of industrial plant

PEK_U05 – can use the tools to model the spreading of chemical contamination

relating to social competences:

PEK_K01 – able to work in a team

PEK_K02 – feels responsible for the results of the tasks entrusted to

PROGRAMME CONTENT

Form of classes - lecture Number

o

f

h

o

u

r

s

Lec

1

Basic concepts. The subject of technical safety, safety perception, the essence of

enterprise security, basic definitions, security scopes, importance of safety as a

guarantee of the existence of an entity, the risk and examples of threats to the

elements of the environment. Risks for the environment. The state of insecurity,

its social and economic effects. Types of security. Examples of technical failures,

the analysis of the causes and effects.

2

Lec

2

Safety-related items. Safety features versus general security companies.

Organisation and management, skills, specificity of manufacturing technology,

infrastructure condition, emergency planning, internal reviews and analysis of

accidents, development of safe work, organisation of operational service posts,

striving for as few nuisance work. Analysis of the causes of industrial accidents.

Characteristics of chemical companies, dangers, hazardous chemical substances.

2

Lec

3

Polish and the European legislation. Environmental law, Directive 67/548/EEC.

Groups of substances and preparations considered dangerous. Explosive

substances (E) oxidizing (O), extremely flammable (F+), flammable (F),

flammable (R10), very toxic (T+), toxic (T), harmful (Xn), corrosive (C), irritant

2

1

0

1

(Xi), sensitizing (R42 and/or R43), carcinogenic (karc..), mutagenic (Muta.), toxic

to reproduction (Repr.), which are dangerous for the environment (N or/and R52,

R53, R59), European Council Directive 96/82/EC, the Convention on the

transboundary effects of industrial accidents, environmental law, Seveso-

enterprises, non-Seveso enterprises, criteria.

Lec

4

Toxic industrial agents, industrial accidents, severe crashes, industrial

contamination. Process safety. Functional safety, safety assessment map. A

comprehensive evaluation of the installation process in the various phases of the

realisation of the investment.

2

Lec

5

Risk assessment methods. Identification of potential threats. HAZard and

OPerability Study (hazard and operability study), its goals, importance, specialty

risks. Keywords, main and auxiliary keywords, installations, design objectives,

deviations from design intent, hazards, parameter, operational problems, the

experts, the process, pairs of keywords in hazards analysis.

2

Lec

6

Examples of HAZOP analysis. Chemical process, the analysis of installation

nodes, HAZOP team of experts, the structure of the team, the team of experts

work scheme, the development of HAZOP report, deviation, deviation result, the

security, the action. Certification of persons carrying out safety circuits, design

and service.

2

Lec

7

The principles of contamination assessment resulted from the industrial

accidents, toxicity, carcinogenicity, principles for the risks evaluation in areas

contaminated as a result of industrial accidents. Exposure-transmission path-

receptor relationship. Elements of the risk assessment procedures, hazard

identification, exposure assessment, dose-response identification, risk assessment,

uncertainty analysis. Health risk, the risk quotient, the risk index.

2

Lec

8

Elimination of the effects of industrial accidents, environment remediation

methods for the areas contaminated as a result of industrial accidents, examples.

Summary. Knowledge check. 1

Total hours 15

Form of classes - class Number of

hours


hours

Lab

1 Determination of the limits of flammability and explosion of chemical

substances

2

Lab

2 Determination of the effects related to the influence of toxic vapours of volatile

substances resulting from industrial accidents

2

Lab

3 Analysis of explosive substances emissions and risks associated with their

spread in the environment

2

Lab

4 Calculation of the level limits of toxic substances during outflow from a tank,

taking into account different topography and atmospheric conditions

2

Lab

5 Analysis of risks related to the emission of toxic substances during the free

evaporation from the open tank

2

Lab

6 Liquefied gas discharge from a pipeline. Hazard analysis and prevention

consultation and the development of exercises.

2

Lab

7

Calculation of the migration limits of dangerous substances and their

concentrations in areas with dense infrastructure

2

1

0

2

Lab

8

Consultations and development of laboratory reports. 1

Total hours 15

TEACHING TOOLS USED

N1. Software EFFECTS 9 to calculate the potential risks arising from industrial accidents

N2. ALOHA software to calculate the effects of emissions of hazardous substances into the

environment

N3. Multimedia presentations

N4. The laboratory test stand





end)

Educational effect


P (lecture) PEK_W01 –

PEK_W06

final test

F (laboratory) PEK_U01 – PEK_U05 reports from the laboratory excercises

P1 (laboratory) = (F1+F2+F3+F4+F5+F6)/6


PRIMARY LITERATURE:

[67] M.Ryng, Bezpieczenstwo techniczne w przemsle chemicznym , WNT Warszawa 1985

[68] Praca zbiorowa, Zapobieganie stratom w przemyśle, Pol. Łódzka, Łódź 1999

[69] W. Pihowicz, Inżynieria bezpieczeństwa technicznego, Problematyka podstawowa, WNT

2009


[39] Granice palności zgodnie z normą PN-EN 720-2, wskaźniki wybuchowości zgodnie z

normą PN-EN26184-2, temperatury zapłonu w tyglu Clevelanda i Pensky’ego Martnsa

[40] Wydawnictwo Ministerstwa Przemysłu Chemicznego pt. "Niebezpieczne materiały

chemiczne - charakterystyka, zagrożenia, ratownictwo" - Biuro Wydawnicze "Chemia"

Warszawa 1989r.


Dr hab. inż. Adam Pawełczyk, [email protected]

1

0

3


SUBJECT

Technical safety


Chemical Technology






Subject



number***

(knowledge)

PEK_W01 K2Atc_W15 C1 Wy1 N3


PEK_W03 K2Atc_W15 C1, C2 Wy3- Wy4 N3

PEK_W04 K2Atc_W15 C2 Wy4- Wy5 N3

PEK_W05 K2Atc_W15 C3 Wy6- Wy7 N3


(skills)

PEK_U01 K2Atc_U17 C3 La1 N4

PEK_U02 K2Atc_U17, S2Atc_W05 C3 La1 – La2 N1

PEK_U03 K2Atc_U17, S2Atc_W05 C3, C4 La3 – La4 N1

PEK_U04 K2Atc_U17, S2Atc_W05 C3, C4 La5 – La6 N1-N2

PEK_U05 K2Atc_U17 C4 La2-La8 N1-N2

(competences)

PEK_K01 K2Atc_K1

Wy1 – Wy8, La1 –

La7 N1-N4



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